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European Journal of Organic Chemistry

First Detection of a Ruthenium–Carbene–Resorc[4]arene Complex During the Progress of a Metathesis Reaction

Published: 27 February 2017

Author(s): Federica Aiello, Federica Balzano, Francesca Ghirga, Ilaria D'Acquarica, Bruno Botta, Gloria Uccello‐Barretta, Deborah Quaglio

For the first time we describe the detection of a ruthenium‐carbene‐resorc[4]arene complex produced, as a key intermediate, during an olefin metathesis reaction carried out on a resorc[4]arene bicyclic olefin with [Ru(=CHPh)Cl2(PCy3)2] Grubbs first‐generation (G1ST) catalyst. The complex was identified by using high‐resolution (600 MHz) 1H, 31P NMR and DOSY spectroscopy, in a non‐invasive fashion. The singlet at δ = 19.98 ppm (1H NMR), attributed to the...

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ChemBioChem

An Exceptionally Selective DNA Cooperatively Binding Two Ca 2+ Ions

Published: 27 February 2017

Author(s): Wenhu Zhou, Runjhun Saran, Po‐Jung Jimmy Huang, Jinsong Ding, Juewen Liu

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Chemistry - A European Journal

A 2D Metal Oxide Nanosheet as an Efficient Additive for Improving Na‐Ion Electrode Activity of Graphene‐Based Nanocomposites

Published: 27 February 2017

Author(s): Boyeon Park, Seung Mi Oh, Xiaoyan Jin, Kanyaporn Adpakpang, Nam‐Suk Lee, Seong‐Ju Hwang

Abstract An efficient way to improve the Na‐ion electrode activity of graphene‐based nanocomposite is developed by employing exfoliated metal oxide nanosheet as an additive. The titanate‐nanosheet‐incorporated Na–SnS2‐reduced graphene oxide (rG‐O) nanocomposites can be synthesized by the electrostatically derived restacking of the colloidal mixture of SnS2, rG‐O, and titanate nanosheets with the Na+ cation. The incorporation of titanate into...

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Chemistry - A European Journal

Site‐Selective Labeling of Native Proteins by a Multicomponent Approach

Published: 27 February 2017

Author(s): Maheshwerreddy Chilamari, Landa Purushottam, Vishal Rai

Abstract Chemical functionalization of proteins is an indispensable tool. Yet, selective labeling of native proteins has been an arduous task. The limited success of chemical methods allows N‐terminus protein labeling, but the examples with side‐chain residues are rare. Herein, we surpass this challenge through a multicomponent transformation that operates under physiological conditions in the presence of a protein, aldehyde,...

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Chemistry - A European Journal

Improved and General Manganese‐Catalyzed N‐Methylation of Aromatic Amines Using Methanol

Published: 27 February 2017

Author(s): Jacob Neumann, Saravanakumar Elangovan, Anke Spannenberg, Kathrin Junge, Matthias Beller

Abstract A novel lutidine‐based manganese PNP‐pincer complex has been synthesized for the selective N‐methylation of aromatic amines with methanol. Using borrowing hydrogen methodology, a selection of differently functionalized aniline derivatives is selectively methylated in good yields.

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Chemistry - A European Journal

Aliphatic C−C Bond Cleavage in α‐Hydroxy Ketones by a Dioxygen‐Derived Nucleophilic Iron–Oxygen Oxidant

Published: 27 February 2017

Author(s): Shrabanti Bhattacharya, Rubina Rahaman, Sayanti Chatterjee, Tapan K. Paine

Abstract A nucleophilic iron–oxygen oxidant, formed in situ in the reaction between an iron(II)–benzilate complex and O2, oxidatively cleaves the aliphatic C−C bonds of α‐hydroxy ketones. In the cleavage reaction, α‐hydroxy ketones without any α‐C−H bond afford a 1:1 mixture of carboxylic acid and ketone. Isotope labeling studies established that one of the oxygen atoms from dioxygen is incorporated into the carboxylic acid product....

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ChemPhysChem

Colloidal Metal Nanoparticles Prepared by Laser Ablation and their Applications

Published: 27 February 2017

Author(s): Jianming Zhang, Jerome Claverie, Mohamed Chaker, Dongling Ma

Abstract This review article highlights the recent advances of the synthesis and application of metal nanoparticles (NPs) fabricated via pulsed laser ablation in liquid (PLAL) phase and also introduces relevant NP formation mechanisms. Although wet‐chemical approaches have been well established to synthesize colloidal metal NPs with various components and structures, some inherent drawbacks, such as reaction residuals and/or...

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ChemPhysChem

Nanosecond Laser‐Assisted Nitrogen Doping of Graphene Oxide Dispersions

Published: 27 February 2017

Author(s): Dejan Kepić, Stefania Sandoval, Ángel Pérez del Pino, Enikö György, Laura Cabana, Belén Ballesteros, Gerard Tobias

Abstract N‐doped reduced graphene oxide (RGO) has been prepared in bulk form by laser irradiation of graphene oxide (GO) dispersed in an aqueous solution of ammonia. A pulsed Nd:YAG laser with emission wavelengths in the infrared (IR) 1064 nm, visible (Vis) 532 nm, and ultraviolet (UV) 266 nm spectral regions was employed for the preparation of the N‐doped RGO samples. Regardless of the laser energy employed, the resulting material...

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ChemPhysChem

How Size Determines the Value of Gold: Economic Aspects of Wet Chemical and Laser‐Based Metal Colloid Synthesis

Published: 27 February 2017

Author(s): Sandra Jendrzej, Bilal Gökce, Matthias Epple, Stephan Barcikowski

Abstract Gold is one of the most valuable materials, and its monetary value is enhanced by size reduction from bullions to colloidal nanoparticles by a factor of 450. Wet‐chemical reduction with subsequent centrifugation and pulsed laser ablation in liquids are frequently used for pure colloidal gold synthesis. Both methods provide similar physicochemical nanoparticle properties, but are very different synthesis techniques. However,...

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ChemMedChem

How Selective are Hsp90 Inhibitors for Cancer Cells over Normal Cells?

Published: 27 February 2017

Author(s): Yao Wang, Yen Chin Koay, Shelli R. McAlpine

Abstract Selectively inhibiting target proteins in cancer cells over normal cells is one of the most critical features of a successful protein inhibitor for clinical applications. By evaluating and comparing the impact of a clinical N‐terminal heat shock protein 90 (Hsp90) inhibitor, AUY922 (luminespib), on Hsp90 inhibition‐associated cellular events in cancer cells versus normal cells, we found that it produces similar phenotype...

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Most-accessed articles from each ChemPubSoc Europe, ACES, and GDCh journal

January 2017

 


Moritz Malischewski, K. Seppelt
Crystal Structure Determination of the Pentagonal‐Pyramidal Hexamethylbenzene Dication C6(CH3)62+ [Communication]
Angew. Chem. Int. Ed. 2017, vol. 56, p. 368

Cassandra M. Joiner, Meghan E. Breen, James Clayton, Anna K. Mapp
A Bifunctional Amino Acid Enables Both Covalent Chemical Capture and Isolation of in Vivo Protein–Protein Interactions [Communication]
ChemBioChem 2016, 10.1002/cbic.201600578

Michael A. Rowan
Brace Yourself! We have New Editorial Board Members! [Editorial]
ChemCatChem 2017, vol. 9, p. 10

Dieter Wöhrle
Kampf‐ und Explosivstoffe [Treffpunkt Forschung]
Chem. Unserer Zeit 2016, vol. 50, p. 369

Rosaria Ciriminna, Mina Ghahremani, Babak Karimi, Mario Pagliaro
Electrochemical Alcohol Oxidation Mediated by TEMPO‐like Nitroxyl Radicals [Review]
ChemistryOpen 2017, vol. 6, p. 5

Mario Bärtsch, Markus Niederberger
The Role of Interfaces in Heterostructures [Minireview]
ChemPlusChem 2017, vol. 82, p. 42

Yang Song, Rui Peng, Dale K. Hensley, Peter V. Bonnesen, Liangbo Liang, Zili Wu, Harry M. Meyer, Miaofang Chi, Cheng Ma, Bobby G. Sumpter, Adam J. Rondinone
High‐Selectivity Electrochemical Conversion of CO2 to Ethanol using a Copper Nanoparticle/N‐Doped Graphene Electrode [Full Paper]
ChemistrySelect 2016, 10.1002/slct.201601169

Florian Ausfelder, Christian Beilmann, Martin Bertau, Sigmar Bräuninger, Angelika Heinzel, Renate Hoer, Wolfram Koch, Falko Mahlendorf, Anja Metzelthin, Marcell Peuckert, Ludolf Plass, Konstantin Räuchle, Martin Reuter, Georg Schaub, Sebastian Schiebahn, Ekkehard Schwab, Ferdi Schüth, Detlef Stolten, Gisa Teßmer, Kurt Wagemann, Karl‐Friedrich Ziegahn
Energiespeicherung als Element einer sicheren Energieversorgung [Übersichtsbeitrag]
Chem. Ing. Tech. 2015, vol. 87, p. 17

Vida Zargar, Morteza Asghari, Amir Dashti
A Review on Chitin and Chitosan Polymers: Structure, Chemistry, Solubility, Derivatives, and Applications [Review]
ChemBioEng Rev. 2015, vol. 2, p. 204

Rasmus Frydendal, Elisa A. Paoli, Brian P. Knudsen, Björn Wickman, Paolo Malacrida, Ifan E. L. Stephens, Ib Chorkendorff
Benchmarking the Stability of Oxygen Evolution Reaction Catalysts: The Importance of Monitoring Mass Losses [Article]
ChemElectroChem 2014, 10.1002/celc.201402262

Jingyu Sun, Yanfeng Zhang, Zhongfan Liu
Direct Chemical Vapor Deposition Growth of Graphene on Insulating Substrates [Focus Review]
ChemNanoMat 2016, vol. 2, p. 9

Andreas Schaate, Pascal Roy, Adelheid Godt, Jann Lippke, Florian Waltz, Michael Wiebcke, Peter Behrens
Modulated Synthesis of Zr‐Based Metal–Organic Frameworks: From Nano to Single Crystals [Full Paper]
Chem. Eur. J. 2011, vol. 17, p. 6643

Kakishi Uno, Taeko Sasaki, Nagisa Sugimoto, Hideto Ito, Taishi Nishihara, Shinya Hagihara, Tetsuya Higashiyama, Narie Sasaki, Yoshikatsu Sato, Kenichiro Itami
Key Structural Elements of Unsymmetrical Cyanine Dyes for Highly Sensitive Fluorescence Turn‐On DNA Probes [Full Paper]
Chem. Asian J. 2016, 10.1002/asia.201601430

Jian Rong, Chuanfa Ni, Jinbo Hu
Metal‐Catalyzed Direct Difluoromethylation Reactions [Focus Review]
Asian J. Org. Chem. 2017, 10.1002/ajoc.201600509

Anneli Nordqvist, Gavin O'Mahony, Maria Fridén‐Saxin, Marlene Fredenwall, Anders Hogner, Kenneth L. Granberg, Anna Aagaard, Stefan Bäckström, Anders Gunnarsson, Tim Kaminski, Yafeng Xue, Anita Dellsén, Eva Hansson, Pia Hansson, Ida Ivarsson, Ulla Karlsson, Krister Bamberg, Majlis Hermansson, Jennie Georgsson, Bo Lindmark, Karl Edman
Structure‐Based Drug Design of Mineralocorticoid Receptor Antagonists to Explore Oxosteroid Receptor Selectivity [Full Paper]
ChemMedChem 2017, vol. 12, p. 50

Chuyang Cheng, J. Fraser Stoddart
Wholly Synthetic Molecular Machines [Minireview]
ChemPhysChem 2016, vol. 17, p. 1780

Matthias Beller, Gabriele Centi, Licheng Sun
Chemistry Future: Priorities and Opportunities from the Sustainability Perspective [Essay]
ChemSusChem 2017, vol. 10, p. 6

Ross J. Marshall, Ross S. Forgan
Postsynthetic Modification of Zirconium Metal‐Organic Frameworks [Microreview]
Eur. J. Inorg. Chem. 2016, 10.1002/ejic.201600394

Clemens Cidarér, Martin Hoffmann, Julian Oelmann, Benedikt Wolfram, Martin Bröring
One‐Pot Preparation of Non‐Symmetric meso‐Aryl‐BODIPYs: Functional Derivatives with Unusual Reactivity [Full Paper]
Eur. J. Org. Chem. 2017, p. 77

Deutscher Lebensmittelchemikertag 2015 in Karlsruhe [Poster]
Lebensmittelchemie 2016, vol. 70, p. 1

Marc Sören Homeyer, Brigitte Duvinage
Ein preiswertes Photometer [Bildung & Gesellschaft]
Nachr. Chem. 2017, vol. 65, p. 63

Matthias Ducci
„Jetzt geht’s rund“ – Redoxreaktionen in Alginatbällchen [Artikel]
CHEMKON 2016, vol. 23, p. 14

Sarah Millar
Tips and Tricks for the Lab: Column Choices
ChemViews Magazine 2012.

Most Cited articles from ChemPubSoc Europe, ACES, and GDCh journals


2015

 


Shoujun Zhu, Qingnan Meng, Lei Wang, Junhu Zhang, Yubin Song, Han Jin, Kai Zhang, Hongchen Sun, Haiyu Wang, Bai Yang
Highly Photoluminescent Carbon Dots for Multicolor Patterning, Sensors, and Bioimaging
Angew. Chem. Int. Ed. 2013, vol. 52, pp. 3953–3957

Naohiko Yoshikai, Ye Wei
Synthesis of Pyrroles, Indoles, and Carbazoles through Transition-Metal-Catalyzed C–H Functionalization [Review]
Asian J. Org. Chem. 2013, vol. 2, pp. 466–478

Yinuo Wu, Jun Wang, Fei Mao, Fuk Yee Kwong
Palladium-Catalyzed Cross-Dehydrogenative Functionalization of C(sp2)–H Bonds [Focus Review]
Chem. Asian J. 2014, vol. 9, pp. 26–47

Konggang Qu, Jiasi Wang, Jinsong Ren, Xiaogang Qu
Carbon Dots Prepared by Hydrothermal Treatment of Dopamine as an Effective Fluorescent Sensing Platform for the Label-Free Detection of Iron(III) Ions and Dopamine [Full Paper]
Chem. Eur. J. 2013, vol. 19, pp. 7243–7249

Philipp Kaiser, Rajabhau Bajirao Unde, Christoph Kern, Andreas Jess
Production of Liquid Hydrocarbons with CO2 as Carbon Source based on Reverse Water-Gas Shift and Fischer-Tropsch Synthesis [Research Article]
Chem. Ing. Tech. 2013, vol. 85, pp. 489–499

Anthony J. Arduengo, Roland Krafczyk
Auf der Suche nach Stabilen Carbenen [Organische Chemie]
Chem. Unserer Zeit 1998, vol. 32, pp. 6–14

Balayeshwanth R. Vummidi, Jawad Alzeer, Nathan W. Luedtke
Fluorescent Probes for G-Quadruplex Structures [Review]
ChemBioChem 2013, vol. 14, pp. 540–558

Ashish Kumar Singh, Qiang Xu
Synergistic Catalysis over Bimetallic Alloy Nanoparticles [Review]
ChemCatChem 2013, vol. 5, pp. 652–676

Xiaosi Zhou, Yu-Guo Guo
Highly Disordered Carbon as a Superior Anode Material for Room-Temperature Sodium-Ion Batteries [Communication]
ChemElectroChem 2014, vol. 1, pp. 83–86

Marc Steinmetz, Stefan Grimme
Benchmark Study of the Performance of Density Functional Theory for Bond Activations with (Ni,Pd)-Based Transition-Metal Catalysts [Full Paper]
ChemistryOpen 2013, vol. 2, pp. 115–124

Lluís Ballell, Robert H. Bates, Rob J. Young, Daniel Alvarez-Gomez, Emilio Alvarez-Ruiz, Vanessa Barroso, Delia Blanco, Benigno Crespo, Jaime Escribano, Rubén González, Sonia Lozano, Sophie Huss, Angel Santos-Villarejo, José Julio Martín-Plaza, Alfonso Mendoza, María José Rebollo-Lopez, Modesto Remuiñan-Blanco, José Luis Lavandera, Esther Pérez-Herran, Francisco Javier Gamo-Benito, José Francisco García-Bustos, David Barros, Julia P. Castro, Nicholas Cammack
Fueling Open-Source Drug Discovery: 177 Small-Molecule Leads against Tuberculosis [Full Paper]
ChemMedChem 2013, vol. 8, pp. 313–321

Peter Politzer, Jane S. Murray
Halogen Bonding: An Interim Discussion [Review]
ChemPhysChem 2013, vol. 14, pp. 278–294

Philipp Scharf, Jens Müller
Nucleic Acids With Metal-Mediated Base Pairs and Their Applications [Review]
ChemPlusChem 2013, vol. 78, pp. 20–34

Volker Hessel, Dana Kralisch, Norbert Kockmann, Timothy Noël, Qi Wang
Novel Process Windows for Enabling, Accelerating, and Uplifting Flow Chemistry [Review]
ChemSusChem 2013, vol. 6, pp. 746–789

Helena J. Shepherd, Gábor Molnár, William Nicolazzi, Lionel Salmon, Azzedine Bousseksou
Spin Crossover at the Nanometre Scale [Microreview]
Eur. J. Inorg. Chem. 2013, pp. 653–661

Junichiro Yamaguchi, Kei Muto, Kenichiro Itami
Recent Progress in Nickel-Catalyzed Biaryl Coupling [Microreview]
Eur. J. Org. Chem. 2013, pp. 19–30

David Schweinfurth, Naina Deibel, Fritz Weisser, Biprajit Sarkar
Mit Klick zu neuen Liganden [Magazin]
Nachr. Chem. 2011, vol. 59, pp. 937–941
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