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Chemistry - A European Journal

From Anilines to Quinolines: Iodide‐ and Silver‐Mediated Aerobic Double C−H Oxidative Annulation–Aromatization

Published: 18 October 2017

Author(s): Jiwei Wu, Zhixiong Liao, Dong Liu, Chien‐Wei Chiang, Zheng Li, Zhonghao Zhou, Hong Yi, Xu Zhang, Zixin Deng, Aiwen Lei

Abstract Quinoline synthesis from easily accessible raw materials such as anilines is a valuable and meaningful task. Herein, we communicate an iodide‐ and silver‐mediated C−H/C−H oxidative annulation–aromatization between anilines and allyl alcohols. This protocol provides a direct route to the synthesis of quinoline derivatives from inexpensive commodities. Various kinds of anilines, even heterocyclic anilines, were shown to be...

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Chemistry - A European Journal

Role of Acid in Tailoring Prussian Blue as Cathode for High‐Performance Sodium‐Ion Battery

Published: 18 October 2017

Author(s): Yang Liu, Gangya Wei, Mengyue Ma, Yun Qiao

Abstract Prussian blue (PB) with concave centers is synthesized successfully through a hydrothermal method with the assistance of acid. In this study, the role of the acid is investigated systematically by adjusting the reaction temperature and time, using different kinds and amounts of acid, and changing the amount of PVP surfactant added. It is found that the acid can not only trigger the chemical reaction to form cubic PB, but...

thumbnail image: Chemistry - A European Journal

Chemistry - A European Journal

NCN‐Coordinating Ligands based on Pyrene Structure with Potential Application in Organic Electronics

Published: 18 October 2017

Author(s): Dawid Zych, Aneta Kurpanik, Aneta Slodek, Anna Maroń, Michał Pająk, Grażyna Szafraniec‐Gorol, Marek Matussek, Stanisław Krompiec, Ewa Schab‐Balcerzak, Sonia Kotowicz, Mariola Siwy, Karolina Smolarek, Sebastian Maćkowski, Witold Danikiewicz

Abstract Five novel derivatives of pyrene, substituted at positions 1,3,6,8 with 4‐(2,2‐dimethylpropyloxy)pyridine (P1), 4‐decyloxypyridine (P2), 4‐pentylpyridine (P3), 1‐decyl‐1,2,3‐triazole (P4), and 1‐benzyl‐1,2,3‐triazole (P5), are obtained through a Suzuki–Miyaura cross‐coupling reaction or CuI‐catalyzed 1,3‐dipolar cycloaddition reaction, respectively, and characterized thoroughly. TGA measurements reveal the high thermal stability of the compounds....

thumbnail image: Chemistry - A European Journal

Chemistry - A European Journal

Solid‐Phase Extraction of Hemoglobin from Human Whole Blood with a Coordination‐Polymer‐Derived Composite Material Based on ZnO and Mesoporous Carbon

Published: 18 October 2017

Author(s): Yuan Jia, Xinxin Xu, Jinzhao Ou, Xiaoxia Liu

Abstract A composite material, ZnO@MC, has been synthesized successfully by calcination using a one‐dimensional zinc‐based coordination polymer as the precursor. In ZnO@MC, ZnO particles with a size of about 5–8 nm are dispersed evenly in a mesoporous carbon matrix. Adsorption experiments at pH 6.8 with 2 mg ZnO@MC as adsorbent illustrated an adsorption efficiency of 92.3 % in 5 mL hemoglobin (Hb) solution with a concentration of...

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ChemMedChem

DNA Microcapsule for Photo‐Triggered Drug Release Systems

Published: 18 October 2017

Author(s): Yukiko Kamiya, Yoshinobu Yamada, Takahiro Muro, Kazunori Matsuura, Hiroyuki Asanuma

Abstract In this study we constructed spherical photo‐responsive microcapsules composed of three photo‐switchable DNA strands. These strands first formed a three‐way junction (TWJ) motif that further self‐assembled to form microspheres through hybridization of the sticky‐end regions of each branch. To serve as the photo‐switch, multiple unmodified azobenzene (Azo) or 2,6‐dimethyl‐4‐(methylthio)azobenzene (SDM‐Azo) were introduced...

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Chemistry - A European Journal

An Fe III Azamacrocyclic Complex as a pH‐Tunable Catholyte and Anolyte for Redox‐Flow Battery Applications

Published: 18 October 2017

Author(s): Pavel B. Tsitovich, Anjula M. Kosswattaarachchi, Matthew R. Crawley, Timothy Y. Tittiris, Timothy R. Cook, Janet R. Morrow

Abstract A reversible Fe3+/Fe2+ redox couple of an azamacrocyclic complex is evaluated as an electrolyte with a pH‐tunable potential range for aqueous redox‐flow batteries (RFBs). The FeIII complex is formed by 1,4,7‐triazacyclononane (TACN) appended with three 2‐methyl‐imidazole donors, denoted as Fe(Tim). This complex exhibits pH‐sensitive redox couples that span E1/2(Fe3+/Fe2+)=317 to −270 mV vs. NHE at pH 3.3 and pH 12.8, respectively. The...

thumbnail image: Chemistry - A European Journal

Chemistry - A European Journal

Concise Total Synthesis of (−)‐Affinisine Oxindole, (+)‐Isoalstonisine, (+)‐Alstofoline, (−)‐Macrogentine, (+)‐ N a ‐Demethylalstonisine, (−)‐Alstonoxine A, and (+)‐Alstonisine

Published: 18 October 2017

Author(s): Michael Rajesh Stephen, M. Toufiqur Rahman, V. V. N. Phani Babu Tiruveedhula, German O. Fonseca, Jeffrey R. Deschamps, James M. Cook

Abstract A highly enantio‐ and diastereoselective strategy to access any member of the sarpagine/macroline family of oxindole alkaloids via internal asymmetric induction was developed from readily available d‐(+)‐tryptophan. At the center of this approach was the diastereospecific generation of the spiro[pyrrolidine‐3,3′‐oxindole] moiety at an early stage via a tert‐butyl hypochlorite‐promoted oxidative rearrangement of a chiral...

thumbnail image: Chemistry - A European Journal

Chemistry - A European Journal

Hybrid Surfactants with N ‐Heterocyclic Carbene Heads as a Multifunctional Platform for Interfacial Catalysis

Published: 18 October 2017

Author(s): Adrian Donner, Kay Hagedorn, Lorenz Mattes, Markus Drechsler, Sebastian Polarz

Abstract Processing of substrates with different solvent compatibility is a persistent problem in homogeneous catalysis, in particular when one starting compound is water soluble and the other is not. A promising concept reported in the literature is micellar catalysis. However, the process of developing catalysts that are surfactants at the same time is still in its early stages. We report the synthesis of a new surfactant system...

thumbnail image: Chemistry - A European Journal

Chemistry - A European Journal

Co 3 O 4 Nanowire Arrays toward Superior Water Oxidation Electrocatalysis in Alkaline Media by Surface Amorphization

Published: 18 October 2017

Author(s): Dan Zhou, Liangbo He, Rong Zhang, Shuai Hao, Xiandeng Hou, Zhiang Liu, Gu Du, Abdullah M. Asiri, Chengbin Zheng, Xuping Sun

Abstract It is highly desirable to develop a simple, fast and straightforward method to boost the alkaline water oxidation of metal oxide catalysts. In this communication, we report our recent finding that the generation of amorphous Co‐borate layer on Co3O4 nanowire arrays supported on Ti mesh (Co3O4@Co‐Bi NA/TM) leads to significantly boosted OER activity. The as‐prepared Co3O4@Co‐Bi NA/TM demands overpotential of 304 mV to drive a geometrical current...

thumbnail image: Chemistry - A European Journal

Chemistry - A European Journal

Octadentate Picolinic Acid‐Based Bispidine Ligand for Radiometal Ions

Published: 17 October 2017

Author(s): Peter Comba, Una Jermilova, Chris Orvig, Brian O. Patrick, Caterina F. Ramogida, Katharina Rück, Christina Schneider, Miriam Starke

Abstract The synthesis of the octadentate bispidine ligand bearing two picolinic acid pendant arms (H2bispa2), and its coordination chemistry with radionuclides relevant for nuclear medicine, namely indium(III) (111In), lutetium(III) (177Lu), and lanthanum(III) (as surrogate for 225Ac), are reported. The non‐radioactive metal complexes of the N6O2‐type bispa ligand were characterized by 1H and 13C NMR spectroscopy, elemental analysis, mass spectrometry and...

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Most-accessed articles from each ChemPubSoc Europe, ACES, and GDCh journal

September 2017

 


Beau P. Pritchett, Etienne J. Donckele, Brian M. Stoltz
Enantioselective Catalysis Coupled with Stereodivergent Cyclization Strategies Enables Rapid Syntheses of (+)-Limaspermidine and (+)-Kopsihainanine A [Communication]
Angew. Chem. Int. Ed. 2017, vol. 56, p. 12624

Joseph Cowell, Matthew Buck, Ali H. Essa, Rebecca Clarke, Waldemar Vollmer, Daniela Vollmer, Catharien M. Hilkens, John D. Isaacs, Michael J. Hall, Joe Gray
Traceless Cleavage of Protein-Biotin Conjugates under Biologically Compatible Conditions [Communication]
ChemBioChem 2017, vol. 18, p. 1688

Isabela C. Man, Hai-Yan Su, Federico Calle-Vallejo, Heine A. Hansen, José I. Martínez, Nilay G. Inoglu, John Kitchin, Thomas F. Jaramillo, Jens K. Nørskov, Jan Rossmeisl
Universality in Oxygen Evolution Electrocatalysis on Oxide Surfaces [Full Paper]
ChemCatChem 2011, vol. 3, p. 1159

Matthias Ducci
Geheimtinten [Artikel]
Chem. Unserer Zeit 2017, vol. 51, p. 228

Balaram Mukhopadhyay, Rituparna Das
Chemical O-Glycosylations: An Overview [Review]
ChemistryOpen 2016, vol. 5, p. 401

Sigma Hashimoto, Takahiro Iwamoto, Daisuke Kurachi, Eiichi Kayahara, Shigeru Yamago
Shortest Double-Walled Carbon Nanotubes Composed of Cycloparaphenylenes [Communication]
ChemPlusChem 2017, vol. 82, p. 1015

Miaofang Chi, Harry M. Meyer, Zili Wu, Liangbo Liang, Peter V. Bonnesen, Dale K. Hensley, Rui Peng, Yang Song, Cheng Ma, Bobby G. Sumpter, Adam J. Rondinone
High-Selectivity Electrochemical Conversion of CO2 to Ethanol using a Copper Nanoparticle/N-Doped Graphene Electrode [Full Paper]
ChemistrySelect 2016, vol. 1, p. 6055

Ekkehard Schwab, Sebastian Schiebahn, Georg Schaub, Martin Reuter, Konstantin Räuchle, Ludolf Plass, Marcell Peuckert, Anja Metzelthin, Falko Mahlendorf, Wolfram Koch, Renate Hoer, Angelika Heinzel, Sigmar Bräuninger, Martin Bertau, Christian Beilmann, Florian Ausfelder, Ferdi Schüth, Detlef Stolten, Gisa Teßmer, Kurt Wagemann, Karl-Friedrich Ziegahn
Energiespeicherung als Element einer sicheren Energieversorgung [Übersichtsbeitrag]
Chem. Ing. Tech. 2015, vol. 87, p. 17

Abas Mohsenzadeh, Akram Zamani, Mohammad J. Taherzadeh
Bioethylene Production from Ethanol: A Review and Techno-economical Evaluation [Review]
ChemBioEng Rev. 2017, vol. 4, p. 75

Andrzej Kapturkiewicz
Electrochemical Generation of Excited Intramolecular Charge-Transfer States [Review]
ChemElectroChem 2017, vol. 4, p. 1604

Yinghui Xue, Qin Zhang, Tao Zhang, Lei Fu
Black Phosphorus: Properties, Synthesis, and Applications in Energy Conversion and Storage [Focus Review]
ChemNanoMat 2017, vol. 3, p. 352

Reto M. Witzig, Dominik Lotter, Vincent C. Fäseke, Christof Sparr
Stereoselective Arene-Forming Aldol Condensation: Catalyst-Controlled Synthesis of Axially Chiral Compounds [Concept]
Chem. Eur. J. 2017, vol. 23, p. 12960

Sandip G. Agalave, Suleman R. Maujan, Vandana S. Pore
Click Chemistry: 1,2,3‐Triazoles as Pharmacophores [Focus Review]
Chem. Asian J. 2011, vol. 6, p. 2696

Jieun Choi, Nagendra Nath Yadav, Hyun-Joon Ha
Front Cover: Preparation of a Stable Bicyclic Aziridinium Ion and Its Ring Expansion toward Piperidines and Azepanes (Asian J. Org. Chem. 9/2017) [Cover Picture]
Asian J. Org. Chem. 2017, vol. 6, p. 1110

Munia F. Sowaileh, Robert A. Hazlitt, David A. Colby
Application of the Pentafluorosulfanyl Group as a Bioisosteric Replacement [Minireview]
ChemMedChem 2017, vol. 12, p. 1481

Thomas J. Penfold, Andrew P. Monkman, Jamie Gibson
The Importance of Vibronic Coupling for Efficient Reverse Intersystem Crossing in Thermally Activated Delayed Fluorescence Molecules [Communication]
ChemPhysChem 2016, vol. 17, p. 2956

Tugba Ozdemir, Yu-Chen Lu, Safacan Kolemen, Esra Tanriverdi-Ecik, Engin U. Akkaya
Generation of Singlet Oxygen by Persistent Luminescent Nanoparticle-Photosensitizer Conjugates: A Proof of Principle for Photodynamic Therapy without Light [Communication]
ChemPhotoChem 2017, vol. 1, p. 183

Junfei Luo, Igor Larrosa
C−H Carboxylation of Aromatic Compounds through CO2 Fixation [Minireview]
ChemSusChem 2017, vol. 10, p. 3317

Ross J. Marshall, Ross S. Forgan
Postsynthetic Modification of Zirconium Metal-Organic Frameworks [Microreview]
Eur. J. Inorg. Chem. 2016, p. 4310

Gregory J. P. Perry, Igor Larrosa
Recent Progress in Decarboxylative Oxidative Cross-Coupling for Biaryl Synthesis [Microreview]
Eur. J. Org. Chem. 2017, p. 3517

Biochemische und molekularbiologische Analytik [Bericht]
Lebensmittelchemie 2017, vol. 71, p. 13

Maren Bulmahn
Parteien zur Wahl [Bildung & Gesellschaft]
Nachr. Chem. 2017, vol. 65, p. 911

Dominique Rosenberg, Svenja Pansegrau, Mirco Wachholz, Alexander Rehling, Maike Busker, Walter Jansen
Redox-Flow-Batterien - Organische Batterien mit Zukunftsperspektiven [Artikel]
CHEMKON 2017, vol. 24, p. 325

Catharina Goedecke
Why Does Iodine Turn Starch Blue?
ChemViews Magazine 2016

Most cited articles from each ChemPubSoc Europe, ACES, and GDCh journal


2016

 


Shoujun Zhu, Qingnan Meng, Lei Wang, Junhu Zhang, Yubin Song, Han Jin, Kai Zhang, Hongchen Sun, Haiyu Wang, Bai Yang
Highly Photoluminescent Carbon Dots for Multicolor Patterning, Sensors, and Bioimaging
Angew. Chem. Int. Ed. 2013, vol. 52, pp. 3953–3957

Balayeshwanth R. Vummidi, Jawad Alzeer, Nathan W. Luedtke
Fluorescent Probes for G-Quadruplex Structures [Review]
ChemBioChem 2013, vol. 14, pp. 540–558

Zhi-Yuan Gu, Jihye Park, Aaron Raiff, Zhangwen Wei, Hong-Cai Zhou
Metal–Organic Frameworks as Biomimetic Catalysts [Minireview]
ChemCatChem 2014, vol. 6, pp. 67–75

Anthony J. Arduengo, Roland Krafczyk
Auf der Suche nach Stabilen Carbenen [Organische Chemie]
Chem. Unserer Zeit 1998, vol. 32, pp. 6–14

Marc Steinmetz, Stefan Grimme
Benchmark Study of the Performance of Density Functional Theory for Bond Activations with (Ni,Pd)-Based Transition-Metal Catalysts [Full Paper]
ChemistryOpen 2013, vol. 2, pp. 115–124

Philipp Scharf, Jens Müller
Nucleic Acids With Metal-Mediated Base Pairs and Their Applications [Review]
ChemPlusChem 2013, vol. 78, pp. 20–34

Philipp Kaiser, Rajabhau Bajirao Unde, Christoph Kern, Andreas Jess
Production of Liquid Hydrocarbons with CO2 as Carbon Source based on Reverse Water-Gas Shift and Fischer-Tropsch Synthesis [Research Article]
Chem. Ing. Tech. 2013, vol. 85, pp. 489–499

Xiaosi Zhou, Yu-Guo Guo
Highly Disordered Carbon as a Superior Anode Material for Room-Temperature Sodium-Ion Batteries [Communication]
ChemElectroChem 2014, vol. 1, pp. 83–86

Chuanxi Wang, Zhenzhu Xu, Chi Zhang
Polyethyleneimine-Functionalized Fluorescent Carbon Dots: Water Stability, pH Sensing, and Cellular Imaging [Full Paper]
ChemNanoMat 2015, vol. 1, pp. 122–127

Konggang Qu, Jiasi Wang, Jinsong Ren, Xiaogang Qu
Carbon Dots Prepared by Hydrothermal Treatment of Dopamine as an Effective Fluorescent Sensing Platform for the Label-Free Detection of Iron(III) Ions and Dopamine [Full Paper]
Chem. Eur. J. 2013, vol. 19, pp. 7243–7249

Yinuo Wu, Jun Wang, Fei Mao, Fuk Yee Kwong
Palladium-Catalyzed Cross-Dehydrogenative Functionalization of C(sp2)–H Bonds [Focus Review]
Chem. Asian J. 2014, vol. 9, pp. 26–47

Naohiko Yoshikai, Ye Wei
Synthesis of Pyrroles, Indoles, and Carbazoles through Transition-Metal-Catalyzed C–H Functionalization [Review]
Asian J. Org. Chem. 2013, vol. 2, pp. 466–478

Lluís Ballell, Robert H. Bates, Rob J. Young, Daniel Alvarez-Gomez, Emilio Alvarez-Ruiz, Vanessa Barroso, Delia Blanco, Benigno Crespo, Jaime Escribano, Rubén González, Sonia Lozano, Sophie Huss, Angel Santos-Villarejo, José Julio Martín-Plaza, Alfonso Mendoza, María José Rebollo-Lopez, Modesto Remuiñan-Blanco, José Luis Lavandera, Esther Pérez-Herran, Francisco Javier Gamo-Benito, José Francisco García-Bustos, David Barros, Julia P. Castro, Nicholas Cammack
Fueling Open-Source Drug Discovery: 177 Small-Molecule Leads against Tuberculosis [Full Paper]
ChemMedChem 2013, vol. 8, pp. 313–321

Peter Politzer, Jane S. Murray
Halogen Bonding: An Interim Discussion [Review]
ChemPhysChem 2013, vol. 14, pp. 278–294

Volker Hessel, Dana Kralisch, Norbert Kockmann, Timothy Noël, Qi Wang
Novel Process Windows for Enabling, Accelerating, and Uplifting Flow Chemistry [Review]
ChemSusChem 2013, vol. 6, pp. 746–789

Helena J. Shepherd, Gábor Molnár, William Nicolazzi, Lionel Salmon, Azzedine Bousseksou
Spin Crossover at the Nanometre Scale [Microreview]
Eur. J. Inorg. Chem. 2013, pp. 653–661

Junichiro Yamaguchi, Kei Muto, Kenichiro Itami
Recent Progress in Nickel-Catalyzed Biaryl Coupling [Microreview]
Eur. J. Org. Chem. 2013, pp. 19–30

David Schweinfurth, Naina Deibel, Fritz Weisser, Biprajit Sarkar
Mit Klick zu neuen Liganden [Magazin]
Nachr. Chem. 2011, vol. 59, pp. 937–941
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A product of ChemPubSoc Europe (16 European Chemical Societies)and Wiley-VCH