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Sustainable Asymmetric Organolithium Chemistry: Enantio‐ and Chemoselective Acylations through Recycling of Solvent, Sparteine, and Weinreb “Amine”

Published: 13 February 2019

Author(s): Serena Monticelli, Wolfgang Holzer, Thierry Langer, Alexander Roller, Berit Olofsson, Vittorio Pace

Abstract The well‐established Hoppe–Beak chemistry, which involves enantioselective generation of organolithium compounds in the presence of (−)‐sparteine, was revisited and applied to unprecedented acylations with Weinreb amides to access highly enantioenriched α‐oxyketones and cyclic α‐aminoketones. Recycling of the sustainable solvent cyclopentyl methyl ether, sparteine, and the released Weinreb “amine” [HNMe(OMe)] was possible through a simple work‐up procedure that enabled full recovery...

thumbnail image: ChemSusChem

Journal of Applied Polymer Science

Curing characteristics and kinetics of EPDM and EOC compounds in co‐vulcanization as blend

Published: 13 February 2019

Author(s): Anoma Thitithammawong, Nattapon Uthaipan, Banja Junhasavasdikul, Charoen Nakason, Ekwipoo Kalkornsurapranee

ABSTRACT Possibility of co‐vulcanization of ethylene octene copolymer (EOC) and ethylene propylene diene terpolymer (EPDM) molecules was studied by assessing the curing characteristic and crosslinking kinetics of EOC and EPDM compounds. Regarding curing, the curing characteristics, cure rate index, and the torque difference (MH − ML) of the EPDM compound are quite similar to those of the EOC compounds at the curing temperature of 180 °C, especially when the EOC octene comonomer content is 5.9...

thumbnail image: Journal of Applied Polymer Science

Journal of Applied Polymer Science

Roles of the molecular weight of n‐ethylene glycol diacrylates and UV irradiance on the mechanical properties at the gel point of acrylic acid based hydrogels

Published: 13 February 2019

Author(s): Saminu M. Magami, Rhodri L. Williams

ABSTRACT We investigated sol–gel transitions in acrylic acid based hydrogels with real time in situ photocrosslinking and Fourier transform mechanical spectroscopy. Crosslinkable n‐ethylene glycol diacrylate (EGDA) compounds with molecular weights (MWs) in the range 171–575 g/mol were used in standard solutions of known polyacrylamide. The mutation number (Nmu) was monitored in all of the experiments, such that Nmu was 0.3 or lower at all of the experimental frequencies. During gelation, a...

thumbnail image: Journal of Applied Polymer Science

Journal of Applied Polymer Science

Alginate–chitosan composite hydrogel film with macrovoids in the inner layer for biomedical applications

Published: 13 February 2019

Author(s): Arindam Banerjee, Somenath Ganguly

ABSTRACT Making of a layered composite using two biopolymer gels with regularly aligned voids in the inner layer is described in this article. Calcium alginate constituted the inner layer, within which voids of 500 μm diameter were embedded in monolayer or in multiple layers using a fluidic device for bubbling. The chitosan without any additional crosslinker was used to form the outer layer. The layered structure enabled compartmentalization of drug hold‐up, and differential release rates....

thumbnail image: Journal of Applied Polymer Science

Helvetica Chimica Acta

Label‐Free Quantification of 5‐Azacytidines Directly in the Genome

Published: 13 February 2019

Author(s): Sarah Schiffers, Thomas M. Wildenhof, Katharina Iwan, Michael Stadlmeier, Markus Müller, Thomas Carell

Abstract Azacytidines (AzaC and AzadC) are clinically relevant pharmaceuticals that operate at the epigenetic level. They are integrated into the genome as antimetabolites to block DNA methylation events. This leads to a reduction of the 5‐methyl‐2′‐deoxycytidine (m5dC) level in the genome, which can activate epigenetically silenced genes. Because of the inherent chemical instability of Aza(d)Cs, their incorporation levels in DNA and RNA are difficult to determine, which hinders correlation of...

thumbnail image: Helvetica Chimica Acta


Thermodynamic Properties of Ammonia Production from Hydrogenation of Alkali and Alkaline Earth Metal Amides

Published: 13 February 2019

Author(s): Qian‐Ru Wang, Ye‐Qin Guan, Wen‐Bo Gao, Jian‐Ping Guo, Ping Chen

Abstract Thermodynamic properties of alkali and alkaline earth metal amides are critical for their performance in hydrogen storage as well as catalytic ammonia synthesis. In this work, the ammonia equilibrium concentrations of LiNH2, KNH2 and Ba(NH2)2 at ca.10 bar of hydrogen pressure and different temperatures were measured by using a high‐pressure gas‐solid reaction system equipped with a conductivity meter. Hydrogenation of KNH2 gives the highest ammonia equilibrium concentration, followed...

thumbnail image: ChemPhysChem

Journal of the Science of Food and Agriculture

The effect of using different types and rates of onion‐water extract in meatball production on the formation of heterocyclic aromatic amines

Published: 13 February 2019

Author(s): Meryem Nuray, Fatih Oz

Abstract BACKGROUND The effect of using different types (yellow, white and purple) and rates (0.25%, 0.50% and 0.75%) of onion‐water extract in meatball production on the various quality criteria of meatballs and the formation of heterocyclic aromatic amines (HCAs) was investigated. RESULTS It was determined that cooking process caused a reduction in the water content of meatballs as well as an increase in pH values. MeIQx, 7,8‐DiMeIQx, 4,8‐DiMeIQx, PhIP, AαC and MeAαC could not be detected in...

thumbnail image: Journal of the Science of Food and Agriculture

Pest Management Science

Post‐harvest management control of Ectomyelois ceratoniae (Zeller) (Lepidoptera: Pyralidae): new insights through essential oil encapsulation in cyclodextrin

Published: 13 February 2019

Author(s): Maha Ben Abada, Soumaya Haouel Hamdi, Riham Gharib, Chokri Messaoud, Sophie Fourmentin, Hélène Greige‐Gerges, Jouda Mediouni Ben Jemâa

Abstract BACKGROUND Essential oils are reported to be bio‐insecticides. However, problems related to their volatility, oxidation and poor water solubility need to be solved before they can be considered as replacement pest control methods. Thus, an appropriate formulation is needed for commercial use. In this work, a new control method based on the use of a powdered cyclodextrin (CD)/1,8‐cineole inclusion complex was assessed against larvae and adults of Ectomyelois ceratoniae (Zeller) in...

thumbnail image: Pest Management Science

Pest Management Science

A novel triple amino acid substitution in the EPSPS found in a high‐level glyphosate‐resistant Amaranthus hybridus population from Argentina

Published: 13 February 2019

Author(s): Valeria E Perotti, Alvaro S Larran, Valeria E Palmieri, Andrea K Martinatto, Clarisa E Alvarez, Daniel Tuesca, Hugo R Permingeat

Abstract Background The evolution of herbicide‐resistant weeds is one of the most important concerns of global agriculture. Amaranthus hybridus L. is a competitive weed for summer crops in South America. In this article, we intend to unravel the molecular mechanisms by which an A. hybridus population from Argentina has become resistant to extraordinarily high levels of glyphosate. Results The glyphosate‐resistant population (A) exhibited particularly high parameters of resistance...

thumbnail image: Pest Management Science

Chemical Engineering & Technology

Direct Coal Liquefaction Using Iron Carbonyl Powder Catalyst

Published: 13 February 2019

Author(s): David Lokhat, Milan Carsky

Abstract Direct coal liquefaction involves catalyzed interactions between molecular hydrogen and coal‐oil slurries at elevated pressure and temperature, typically in the presence of an iron‐based catalyst. Iron carbonyl powder as an alternative first‐stage catalyst was investigated. A series of experimental tests under mild liquefaction conditions were carried out with a high‐pressure batch reactor in order to compare the performance of the iron carbonyl precursor to the traditional superfine...

thumbnail image: Chemical Engineering & Technology

Most-accessed articles from each ChemPubSoc Europe, ACES, and GDCh journal

September 2018


Runze Mao, Jonathan Balon, Xile Hu
Decarboxylative C(sp3)−O Cross-Coupling [Communication]
Angew. Chem. Int. Ed. 2018, vol. 57, p. 13624

Klaus F. Wagenbauer, Floris A. S. Engelhardt, Evi Stahl, Vera K. Hechtl, Pierre Stömmer, Fabian Seebacher, Letizia Meregalli, Philip Ketterer, Thomas Gerling, Hendrik Dietz
How We Make DNA Origami [Concept]
ChemBioChem 2017, vol. 18, p. 1873

Isabela C. Man, Hai-Yan Su, Federico Calle-Vallejo, Heine A. Hansen, José I. Martínez, Nilay G. Inoglu, John Kitchin, Thomas F. Jaramillo, Jens K. Nørskov, Jan Rossmeisl
Universality in Oxygen Evolution Electrocatalysis on Oxide Surfaces [Full Paper]
ChemCatChem 2011, vol. 3, p. 1159

Matthias Epple, Joachim Enax
Moderne Zahnpflege aus chemischer Sicht [Artikel]
Chem. Unserer Zeit 2018, vol. 52, p. 218

Balaram Mukhopadhyay, Rituparna Das
Chemical O-Glycosylations: An Overview [Review]
ChemistryOpen 2016, vol. 5, p. 401

Lei Han, Meng-Ke Wu, Fei-Yan Yi, Dongxiao Chen, Hai-Long Jiang
Chemical Sensors Based on Metal-Organic Frameworks [Review]
ChemPlusChem 2016, vol. 81, p. 675

Miaofang Chi, Harry M. Meyer, Zili Wu, Liangbo Liang, Peter V. Bonnesen, Dale K. Hensley, Rui Peng, Yang Song, Cheng Ma, Bobby G. Sumpter, Adam J. Rondinone
High-Selectivity Electrochemical Conversion of CO2 to Ethanol using a Copper Nanoparticle/N-Doped Graphene Electrode [Full Paper]
ChemistrySelect 2016, vol. 1, p. 6055

Peter Buchholz, Torsten Brandenburg
Demand, Supply, and Price Trends for Mineral Raw Materials Relevant to the Renewable Energy Transition Wind Energy, Solar Photovoltaic Energy, and Energy Storage [Review]
Chem. Ing. Tech. 2018, vol. 90, p. 141

Abas Mohsenzadeh, Akram Zamani, Mohammad J. Taherzadeh
Bioethylene Production from Ethanol: A Review and Techno-economical Evaluation [Review]
ChemBioEng Rev. 2017, vol. 4, p. 75

Lantao Liu, Yanli Zhou, Shuang Liu, Maotian Xu
The Applications of Metal−Organic Frameworks in Electrochemical Sensors [Review]
ChemElectroChem 2018, vol. 5, p. 6

Hejin Jiang, Li Zhang, Minghua Liu
Self-Assembly of 1D Helical Nanostructures into Higher Order Chiral Nanostructures in Supramolecular Systems [Focus Review]
ChemNanoMat 2018, vol. 4, p. 720

Sa Xiao, Yi Lu, Xin Li, Bing-Yu Xiao, Liang Wu, Jian-Ping Song, Yu-Xuan Xiao, Si-Ming Wu, Jie Hu, Yong Wang, Gang-Gang Chang, Ge Tian, Silvia Lenaerts, Christoph Janiak, Xiao-Yu Yang, Bao-Lian Su
Hierarchically Dual-Mesoporous TiO2 Microspheres for Enhanced Photocatalytic Properties and Lithium Storage [Full Paper]
Chem. Eur. J. 2018, vol. 24, p. 13246

Sandip G. Agalave, Suleman R. Maujan, Vandana S. Pore
Click Chemistry: 1,2,3‐Triazoles as Pharmacophores [Focus Review]
Chem. Asian J. 2011, vol. 6, p. 2696

Michael C. Willis, Edward J. Emmett
The Development and Application of Sulfur Dioxide Surrogates in Synthetic Organic Chemistry [Focus Review]
Asian J. Org. Chem. 2015, vol. 4, p. 602

Hartmut Beck, Mario Jeske, Kai Thede, Friederike Stoll, Ingo Flamme, Metin Akbaba, Jens-Kerim Ergüden, Gunter Karig, Jörg Keldenich, Felix Oehme, Hans-Christian Militzer, Ingo V. Hartung, Uwe Thuss
Discovery of Molidustat (BAY 85-3934): A Small-Molecule Oral HIF-Prolyl Hydroxylase (HIF-PH) Inhibitor for the Treatment of Renal Anemia [Full Paper]
ChemMedChem 2018, vol. 13, p. 988

Gloria Tabacchi
Supramolecular Organization in Confined Nanospaces [Review]
ChemPhysChem 2018, vol. 19, p. 1249

Baokun Qiao, Zhiyong Jiang
Catalytic Photoreduction Induced by Visible Light [Minireview]
ChemPhotoChem 2018, vol. 2, p. 703

Xinyue Zhang, Mingyue Jiang, Na Niu, Zhijun Chen, Shujun Li, Shouxin Liu, Jian Li
Natural-Product-Derived Carbon Dots: From Natural Products to Functional Materials [Review]
ChemSusChem 2018, vol. 11, p. 11

Ross J. Marshall, Ross S. Forgan
Postsynthetic Modification of Zirconium Metal-Organic Frameworks [Microreview]
Eur. J. Inorg. Chem. 2016, p. 4310

Luca Capaldo, Davide Ravelli
Hydrogen Atom Transfer (HAT): A Versatile Strategy for Substrate Activation in Photocatalyzed Organic Synthesis [Microreview]
Eur. J. Org. Chem. 2017, p. 2056

Cover Picture Lebensmittelchemie 4/2018 [Cover Picture]
Lebensmittelchemie 2018, vol. 72

Thomas U. Probst
Umbrüche beim Kunststoffrecycling [Industrie & Technik]
Nachr. Chem. 2018, vol. 66, p. 868

Alexander Engl, Alexandra Schmelzer, Björn Risch
Chemie Pur - Unterrichten in der Natur: Ätherischen Ölen auf der Spur [Artikel]
CHEMKON 2018, vol. 25, p. 7

Catharina Goedecke
Why Does Iodine Turn Starch Blue?
ChemViews Magazine 2016

Most cited articles from each ChemPubSoc Europe, ACES, and GDCh journal



Eric J. Popczun, Carlos G. Read, Christopher W. Roske, Nathan S. Lewis, Raymond E. Schaak
Highly Active Electrocatalysis of the Hydrogen Evolution Reaction by Cobalt Phosphide Nanoparticles
Angew. Chem. Int. Ed. 2014, vol. 53, pp. 5427–5430

Philippe Compain, Anne Bodlenner
The Multivalent Effect in Glycosidase Inhibition: A New, Rapidly Emerging Topic in Glycoscience [Minireview]
ChemBioChem 2014, vol. 15, pp. 1239–1251

Zhi-Yuan Gu, Jihye Park, Aaron Raiff, Zhangwen Wei, Hong-Cai Zhou
Metal–Organic Frameworks as Biomimetic Catalysts [Minireview]
ChemCatChem 2014, vol. 6, pp. 67–75

Anthony J. Arduengo, Roland Krafczyk
Auf der Suche nach Stabilen Carbenen [Organische Chemie]
Chem. Unserer Zeit 1998, vol. 32, pp. 6–14

Félix Sancenón, Lluís Pascual, Mar Oroval, Elena Aznar, Ramón Martínez-Máñez
Gated Silica Mesoporous Materials in Sensing Applications [Review]
ChemistryOpen 2015, vol. 4, pp. 418–437

Jun Pu, Tingting Wang, Haiyang Wang, Yao Tong, Chenchen Lu, Wei Kong, Zhenghua Wang
Direct Growth of NiCo2S4 Nanotube Arrays on Nickel Foam as High-Performance Binder-Free Electrodes for Supercapacitors [Full Paper]
ChemPlusChem 2014, vol. 79, pp. 577–583

Francisco Trespalacios, Ignacio E. Grossmann
Review of Mixed-Integer Nonlinear and Generalized Disjunctive Programming Methods [Review]
Chemie Ingenieur Technik 2014, vol. 86, pp. 991–1012

Xiaosi Zhou, Yu-Guo Guo
Highly Disordered Carbon as a Superior Anode Material for Room-Temperature Sodium-Ion Batteries [Communication]
ChemElectroChem 2014, vol. 1, pp. 83–86

Chuanxi Wang, Zhenzhu Xu, Chi Zhang
Polyethyleneimine-Functionalized Fluorescent Carbon Dots: Water Stability, pH Sensing, and Cellular Imaging [Full Paper]
ChemNanoMat 2015, vol. 1, pp. 122–127

Matthew N. Hopkinson, Basudev Sahoo, Jun-Long Li, Frank Glorius
Dual Catalysis Sees the Light: Combining Photoredox with Organo-, Acid, and Transition-Metal Catalysis [Minireview]
Chemistry – A European Journal 2014, vol. 20, pp. 3874–3886

Yinuo Wu, Jun Wang, Fei Mao, Fuk Yee Kwong
Palladium-Catalyzed Cross-Dehydrogenative Functionalization of C(sp2)–H Bonds [Focus Review]
Chemistry – An Asian Journal 2014, vol. 9, pp. 26–47

Derong Cao, Herbert Meier
Pillar[n]arenes—a Novel, Highly Promising Class of Macrocyclic Host Molecules [Focus Review]
Asian Journal of Organic Chemistry 2014, vol. 3, pp. 244–262

Daniel Gallenkamp, Kathy A. Gelato, Bernard Haendler, Hilmar Weinmann
Bromodomains and Their Pharmacological Inhibitors [Review]
ChemMedChem 2014, vol. 9, pp. 438–464

Antonio Bauzá, Tiddo J. Mooibroek, Antonio Frontera
The Bright Future of Unconventional σ/π-Hole Interactions [Review]
ChemPhysChem 2015, vol. 16, pp. 2496–2517

Ksenia S. Egorova, Valentine P. Ananikov
Toxicity of Ionic Liquids: Eco(cyto)activity as Complicated, but Unavoidable Parameter for Task-Specific Optimization [Review]
ChemSusChem 2014, vol. 7, pp. 336–360

Shunichi Fukuzumi, Dachao Hong
Homogeneous versus Heterogeneous Catalysts in Water Oxidation [Microreview]
Eur. J. Inorg. Chem. 2014, pp. 645–659

Fabien Toulgoat, Sébastien Alazet, Thierry Billard
Direct Trifluoromethylthiolation Reactions: The “Renaissance” of an Old Concept [Microreview]
Eur. J. Org. Chem. 2014, pp. 2415–2428

David Schweinfurth, Naina Deibel, Fritz Weisser, Biprajit Sarkar
Mit Klick zu neuen Liganden [Magazin]
Nachr. Chem. 2011, vol. 59, pp. 937–941

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