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Journal of Raman Spectroscopy

Detection of saliva morphine using surface‐enhanced Raman spectroscopy combined with immunochromatographic assay

Published: 17 January 2020

Author(s): Wei Li, Xiaozhou Li, Tianyue Yang, Xingjia Guo, Youtao Song

Abstract An immunochromatographic assay (ICA) based on surface‐enhanced Raman scattering (SERS) method was developed for the detection of morphine in this study. Indirect competitive immunoadsorption was adopted in the ICA due to the small molecular weight of morphine. Antibody modified gold nanoparticles in the ICA were labeled with Raman reporters and were used as the SERS enhancement substrate. By measuring the feature peaks of Raman reporter MBA at 1,078 cm−1, a quantitative estimation of...

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Journal of the American Ceramic Society

Single‐step densification of nanocrystalline CeO2 by the cold sintering process

Published: 17 January 2020

Author(s): Clive A. Randall, Scott T. Misture, Jonathan Perini, Sun Hwi Bang, Zhongming Fan, Kosuke Tsuji, Arnaud Ndayishimiye, Thomasina H. Zaengle

Abstract This study reports the successful single‐step cold sintering of nanocrystalline cerium dioxide (CeO2) at temperatures ranging from 250°C to 400°C under 500 MPa, using molten hydroxides flux solvents. CeO2 ceramics obtained were 82 to 91% of the theoretical density. Structural and microstructural investigations of the as‐cold sintered CeO2 ceramics were conducted to further understand this new approach to cold sinter ceramics. Electrical conductivity measured by two‐point AC impedance...

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Advanced Functional Materials

Three Electron Reversible Redox Reaction in Sodium Vanadium Chromium Phosphate as a High‐Energy‐Density Cathode for Sodium‐Ion Batteries

Published: 17 January 2020

Author(s): John B. Goodenough, Haibo Jin, Hongcai Gao, Xiangwen Gao, Yongjie Zhao

Abstract A sodium‐ion battery operating at room temperature is of great interest for large‐scale stationary energy storage because of its intrinsic cost advantage. However, the development of a high capacity cathode with high energy density remains a great challenge. In this work, sodium super ionic conductor‐structured Na3V2−xCrx(PO4)3 is achieved through the sol–gel method; Na3V1.5Cr0.5(PO4)3 is demonstrated to have a capacity of 150 mAh g−1 with reversible three‐electron redox reactions...

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Advanced Materials

3D‐Printed Structure Boosts the Kinetics and Intrinsic Capacitance of Pseudocapacitive Graphene Aerogels

Published: 17 January 2020

Author(s): Bin Yao, Swetha Chandrasekaran, Haozhe Zhang, Annie Ma, Junzhe Kang, Lei Zhang, Xihong Lu, Fang Qian, Cheng Zhu, Eric B. Duoss, Christopher M. Spadaccini, Marcus A. Worsley, Yat Li

Abstract The performance of pseudocapacitive electrodes at fast charging rates are typically limited by the slow kinetics of Faradaic reactions and sluggish ion diffusion in the bulk structure. This is particularly problematic for thick electrodes and electrodes highly loaded with active materials. Here, a surface‐functionalized 3D‐printed graphene aerogel (SF‐3D GA) is presented that achieves not only a benchmark areal capacitance of 2195 mF cm−2 at a high current density of 100 mA cm−2 but...

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European Journal of Organic Chemistry

Nitrene Transfer Reactions for Asymmetric C–H Amination: Recent Development

Published: 17 January 2020

Author(s): Hiroki Hayashi, Tatsuya Uchida

C–H bonds are ubiquitous and abundant in organic molecules. If C–H bonds could be directly converted to desired functional groups in a chemo‐, site‐, and stereoselective manner, C–H functionalization would be a strong and useful tool for organic synthesis. Recent developments in catalytic and enzymatic chemistry have achieved highly sustainable and selective nitrene C–H insertion. Initially, C–H amination was inspired by model studies on enzymatic oxidation and used iminoiodinanes, nitrogen...

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European Journal of Organic Chemistry

Three Step Synthesis of Fully and Differently Arylated Pyridines

Published: 17 January 2020

Author(s): Mao Arita, Soichi Yokoyama, Haruyasu Asahara, Nagatoshi Nishiwaki

Condensation of β‐(2‐pyridyl)enamine and α,β‐unsaturated ketone in the presence of FeCl3 under air afforded highly substituted pyridines. In this transformation, FeCl3 acted as not only an acid catalyst but also an oxidant for the intermediate dihydropyridine. The substituents could be easily modified by altering the substrates to obtain tri‐ and tetraarylpyridines including bipyridines and terpyridine. Synthesis of differently substituted pentaarylpyridines was consequently achieved via only...

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Advanced Materials

Hydration‐Effect‐Promoting Ni–Fe Oxyhydroxide Catalysts for Neutral Water Oxidation

Published: 17 January 2020

Author(s): Ning Wang, Zhen Cao, Xueli Zheng, Bo Zhang, Sergey M. Kozlov, Peining Chen, Chengqin Zou, Xiangbin Kong, Yunzhou Wen, Min Liu, Yansong Zhou, Cao Thang Dinh, Lirong Zheng, Huisheng Peng, Ying Zhao, Luigi Cavallo, Xiaodan Zhang, Edward H. Sargent

Abstract Oxygen evolution reaction (OER) catalysts that function efficiently in pH‐neutral electrolyte are of interest for biohybrid fuel and chemical production. The low concentration of reactant in neutral electrolyte mandates that OER catalysts provide both the water adsorption and dissociation steps. Here it is shown, using density functional theory simulations, that the addition of hydrated metal cations into a Ni–Fe framework contributes water adsorption functionality proximate to the...

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Energy Technology

Solid versus Liquid—A Bottom‐Up Calculation Model to Analyze the Manufacturing Cost of Future High‐Energy Batteries

Published: 17 January 2020

Author(s): Gunther Reinhart, Anna Julia Imbsweiler, Heiko Knörzer, Joscha Schnell

All‐solid‐state batteries (ASSB) are promising candidates for future energy storage. However, only a little is known about the manufacturing costs for industrial production. Herein, a detailed bottom‐up calculation is performed to estimate the required investment and to facilitate comparison with conventional lithium‐ion batteries (LIB). Results indicate that sulfide‐based ASSBs can indeed be competitive if the material compatibility issues can be solved and production is successfully scaled....

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International Journal of Applied Ceramic Technology

Nanofibers reinforced silica aerogel composites having flexibility and ultra‐low thermal conductivity

Published: 17 January 2020

Author(s): Rubing Zhang, Zhimin An, Yue Zhao, Liang Zhang, Peng Zhou

Abstract For the sake of enhancing the performance of flexible silica aerogel in practical applications, flexible SiO2/SnO2 nanofibers (SSNF) reinforced flexible silica aerogel composites (abbreviated as SiO2‐SSNF) were successfully prepared. Firstly, the SiO2/SnO2 nanofibers with fine diameter (~320 nm) and excellent flexibility were prepared by electrospinning technology. Then the aerogel composites were synthesized by adding the flexible SSNF to the silica solution and through the sol‐gel...

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Journal of the American Ceramic Society

Crystal structure, phonon modes, and bond characteristics of AgPb2B2V3O12 (B = Mg, Zn) microwave ceramics

Published: 17 January 2020

Author(s): Rakhi Madhuri, Subodh Ganesanpotti

Abstract AgPb2B2V3O12 (B = Mg, Zn) ceramics with low sintering temperature were synthesized via the conventional solid‐state reaction route. Rietveld refinements of the X‐ray diffraction patterns confirm cubic symmetry with space group . The number of observed vibrational modes and those predicted by group theoretical calculations also confirm the space group. At the optimum sintering temperature of 750°C/4 hours, AgPb2Mg2V3O12 has a relative permittivity of 23.3 ± 0.2, unloaded quality factor...

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Most-accessed articles from each ChemPubSoc Europe, ACES, and GDCh journal

December 2019


Duanyang Kong, Patrick J. Moon, Odey Bsharat, Rylan J. Lundgren
Direct Catalytic Decarboxylative Amination of Aryl Acetic Acids [Research Article]
Angew. Chem. Int. Ed. 2020, vol. 59, no. 3, p. 1313

Bing Liu, Lihui He, Liping Wang, Tao Li, Changcheng Li, Huayi Liu, Yunzi Luo, Rui Bao
Protein Crystallography and Site-Direct Mutagenesis Analysis of the Poly(ethylene terephthalate) Hydrolase PETase from Ideonella sakaiensis [Communication]
ChemBioChem 2018, vol. 19, no. 14, p. 1471

Isabela C. Man, Hai-Yan Su, Federico Calle-Vallejo, Heine A. Hansen, José I. Martínez, Nilay G. Inoglu, John Kitchin, Thomas F. Jaramillo, Jens K. Nørskov, Jan Rossmeisl
Universality in Oxygen Evolution Electrocatalysis on Oxide Surfaces [Full Paper]
ChemCatChem 2011, vol. 3, no. 7, p. 1159

Wolfgang Pfeiffer, Van Than Nguyen, Jan Neumann, Dirk Awe, Jens Tränckner
Operation and Control of a Full-Scale Biogas Plant Treating Wastewater from the Cleaning of Car Tanks [Research Article]
Chem. Eng. Technol. 2020, vol. 43, no. 1, p. 84

Dieter Wöhrle
Kunststoffe [Artikel]
Chem. Unserer Zeit 2019, vol. 53, no. 1, p. 50

Luling Wu, Xue Tian, Hai-Hao Han, Jie Wang, Robin R. Groleau, Paramabhorn Tosuwan, Boontana Wannalerse, Adam C. Sedgwick, Steven D. Bull, Xiao-Peng He, Tony D. James
A Simple Near-Infrared Fluorescent Probe for the Detection of Peroxynitrite [Communication]
ChemistryOpen 2019, vol. 8, no. 12, p. 1407

Daewoo Han, Andrew J. Steckl
Coaxial Electrospinning Formation of Complex Polymer Fibers and their Applications [Review]
ChemPlusChem 2019, vol. 84, no. 10, p. 1453

Miaofang Chi, Harry M. Meyer, Zili Wu, Liangbo Liang, Peter V. Bonnesen, Dale K. Hensley, Rui Peng, Yang Song, Cheng Ma, Bobby G. Sumpter, Adam J. Rondinone
High-Selectivity Electrochemical Conversion of CO2 to Ethanol using a Copper Nanoparticle/N-Doped Graphene Electrode [Full Paper]
ChemistrySelect 2016, vol. 1, no. 19, p. 6055

Ekkehard Schwab, Sebastian Schiebahn, Georg Schaub, Martin Reuter, Konstantin Räuchle, Ludolf Plass, Marcell Peuckert, Anja Metzelthin, Falko Mahlendorf, Wolfram Koch, Renate Hoer, Angelika Heinzel, Sigmar Bräuninger, Martin Bertau, Christian Beilmann, Florian Ausfelder, Ferdi Schüth, Detlef Stolten, Gisa Teßmer, Kurt Wagemann, Karl-Friedrich Ziegahn
Energiespeicherung als Element einer sicheren Energieversorgung [Übersichtsbeitrag]
Chem. Ing. Tech. 2015, vol. 87, no. 1-2, p. 17

Abas Mohsenzadeh, Akram Zamani, Mohammad J. Taherzadeh
Bioethylene Production from Ethanol: A Review and Techno-economical Evaluation [Review]
ChemBioEng Rev. 2017, vol. 4, no. 2, p. 75

Lucia Mazzapioda, Carmelo Lo Vecchio, Annalisa Paolone, Antonino Salvatore Aricò, Vincenzo Baglio, Maria Assunta Navarra
Enhancing Oxygen Reduction Reaction Catalytic Activity Using a Sub-Stoichiometric CaTiO3−δ Additive [Cover Profile]
ChemElectrochem 2019, vol. 6, no. 24, p. 5910

S. Ghosh, B. Pradhan
Lead-Free Metal Halide Perovskite Nanocrystals: Challenges, Applications, and Future Aspects [Minireview]
ChemNanoMat 2019, vol. 5, no. 3, p. 300

Frank Tabellion, Christoph Peters, Uwe Fischbeck, Manfred Regitz, Fritz Preuss
Imidovanadium(V) Complexes as Reaction Partners for Kinetically Stabilized Phosphaalkynes: Synthesis of 1,2,4‐Azaphosphavanada(V)‐cyclobutenes, 1,3,5‐Triphosphabenzenes, and 1H‐1,2,4‐Azadiphospholes [Organophosphorus Compounds, Part 148 : Full Paper]
Chem. Eur. J. 2000, vol. 6, no. 24, p. 4558

Byunghyuck Jung, Jungkyu K. Lee, Jungnam Kim, Eunhye K. Kang, Sang Yeong Han, Hee-Yoon Lee, Insung S. Choi
Synthetic Strategies for (−)-Cannabidiol and Its Structural Analogs [Minireview]
Chem. Asian J. 2019, vol. 14, no. 21, p. 3749

Arun K. Sinha, Danish Equbal
Thiol−Ene Reaction: Synthetic Aspects and Mechanistic Studies of an Anti-Markovnikov-Selective Hydrothiolation of Olefins [Focus Review]
Asian J. Org. Chem. 2019, vol. 8, no. 1, p. 32

Avick Kumar Ghosh, Indranil Samanta, Anushree Mondal, Wenshe Ray Liu
Covalent Inhibition in Drug Discovery [Review]
ChemMedChem 2019, vol. 14, no. 9, p. 889

Andrea Álvarez, Marta Borges, Juan José Corral-Pérez, Joan Giner Olcina, Lingjun Hu, Damien Cornu, Rui Huang, Dragos Stoian, Atsushi Urakawa
CO2 Activation over Catalytic Surfaces [Concept]
ChemPhysChem 2017, vol. 18, no. 22, p. 3135

Matthias Freitag, Nadja Möller, Andreas Rühling, Cristian A. Strassert, Bart Jan Ravoo, Frank Glorius
Photocatalysis in the Dark: Near-Infrared Light Driven Photoredox Catalysis by an Upconversion Nanoparticle/Photocatalyst System [Communication]
ChemPhotoChem 2019, vol. 3, no. 1, p. 24

Mingshuai Ma, Lin Dai, Chuanling Si, Lanfeng Hui, Zhong Liu, Yonghao Ni
Front Cover: A Facile Preparation of Super Long-Term Stable Lignin Nanoparticles from Black Liquor (ChemSusChem 24/2019) [Cover Picture]
ChemSusChem 2019, vol. 12, no. 24, p. 5213

Stephen A. Matlin, Goverdhan Mehta, Henning Hopf, Alain Krief
The Periodic Table of the Chemical Elements and Sustainable Development [Essay]
Eur. J. Inorg. Chem. 2019, p. 4170

Luca Capaldo, Davide Ravelli
Hydrogen Atom Transfer (HAT): A Versatile Strategy for Substrate Activation in Photocatalyzed Organic Synthesis [Microreview]
Eur. J. Org. Chem. 2017, p. 2056

Cover Picture Lebensmittelchemie 6/2019 [Cover Picture]
Lebensmittelchemie 2019, vol. 73, no. 6

Elementerätsel 1 [Wissenschaft + Forschung]
Nachr. Chem. 2019, vol. 67, no. 12, p. 40

Schüleraufgabe: CHEMKON 2/2017 [Schüleraufgabe]
CHEMKON 2017, vol. 24, no. 2, p. 91

Zheng Ma, Douglas R. MacFarlane, Mega Kar
Mg Cathode Materials and Electrolytes for Rechargeable Mg Batteries: A Review [Minireview]
Batteries & Supercaps 2019, vol. 2, no. 2, p. 115

Catharina Goedecke
Why Does Iodine Turn Starch Blue?
ChemViews Magazine 2016

Most cited articles from each ChemPubSoc Europe, ACES, and GDCh journal



Eric J. Popczun, Carlos G. Read, Christopher W. Roske, Nathan S. Lewis, Raymond E. Schaak
Highly Active Electrocatalysis of the Hydrogen Evolution Reaction by Cobalt Phosphide Nanoparticles
Angew. Chem. Int. Ed. 2014, vol. 53, pp. 5427–5430

Philippe Compain, Anne Bodlenner
The Multivalent Effect in Glycosidase Inhibition: A New, Rapidly Emerging Topic in Glycoscience [Minireview]
ChemBioChem 2014, vol. 15, pp. 1239–1251

Zhi-Yuan Gu, Jihye Park, Aaron Raiff, Zhangwen Wei, Hong-Cai Zhou
Metal–Organic Frameworks as Biomimetic Catalysts [Minireview]
ChemCatChem 2014, vol. 6, pp. 67–75

Anthony J. Arduengo, Roland Krafczyk
Auf der Suche nach Stabilen Carbenen [Organische Chemie]
Chem. Unserer Zeit 1998, vol. 32, pp. 6–14

Félix Sancenón, Lluís Pascual, Mar Oroval, Elena Aznar, Ramón Martínez-Máñez
Gated Silica Mesoporous Materials in Sensing Applications [Review]
ChemistryOpen 2015, vol. 4, pp. 418–437

Jun Pu, Tingting Wang, Haiyang Wang, Yao Tong, Chenchen Lu, Wei Kong, Zhenghua Wang
Direct Growth of NiCo2S4 Nanotube Arrays on Nickel Foam as High-Performance Binder-Free Electrodes for Supercapacitors [Full Paper]
ChemPlusChem 2014, vol. 79, pp. 577–583

Francisco Trespalacios, Ignacio E. Grossmann
Review of Mixed-Integer Nonlinear and Generalized Disjunctive Programming Methods [Review]
Chemie Ingenieur Technik 2014, vol. 86, pp. 991–1012

Xiaosi Zhou, Yu-Guo Guo
Highly Disordered Carbon as a Superior Anode Material for Room-Temperature Sodium-Ion Batteries [Communication]
ChemElectroChem 2014, vol. 1, pp. 83–86

Chuanxi Wang, Zhenzhu Xu, Chi Zhang
Polyethyleneimine-Functionalized Fluorescent Carbon Dots: Water Stability, pH Sensing, and Cellular Imaging [Full Paper]
ChemNanoMat 2015, vol. 1, pp. 122–127

Matthew N. Hopkinson, Basudev Sahoo, Jun-Long Li, Frank Glorius
Dual Catalysis Sees the Light: Combining Photoredox with Organo-, Acid, and Transition-Metal Catalysis [Minireview]
Chemistry – A European Journal 2014, vol. 20, pp. 3874–3886

Yinuo Wu, Jun Wang, Fei Mao, Fuk Yee Kwong
Palladium-Catalyzed Cross-Dehydrogenative Functionalization of C(sp2)–H Bonds [Focus Review]
Chemistry – An Asian Journal 2014, vol. 9, pp. 26–47

Derong Cao, Herbert Meier
Pillar[n]arenes—a Novel, Highly Promising Class of Macrocyclic Host Molecules [Focus Review]
Asian Journal of Organic Chemistry 2014, vol. 3, pp. 244–262

Daniel Gallenkamp, Kathy A. Gelato, Bernard Haendler, Hilmar Weinmann
Bromodomains and Their Pharmacological Inhibitors [Review]
ChemMedChem 2014, vol. 9, pp. 438–464

Antonio Bauzá, Tiddo J. Mooibroek, Antonio Frontera
The Bright Future of Unconventional σ/π-Hole Interactions [Review]
ChemPhysChem 2015, vol. 16, pp. 2496–2517

Ksenia S. Egorova, Valentine P. Ananikov
Toxicity of Ionic Liquids: Eco(cyto)activity as Complicated, but Unavoidable Parameter for Task-Specific Optimization [Review]
ChemSusChem 2014, vol. 7, pp. 336–360

Shunichi Fukuzumi, Dachao Hong
Homogeneous versus Heterogeneous Catalysts in Water Oxidation [Microreview]
Eur. J. Inorg. Chem. 2014, pp. 645–659

Fabien Toulgoat, Sébastien Alazet, Thierry Billard
Direct Trifluoromethylthiolation Reactions: The “Renaissance” of an Old Concept [Microreview]
Eur. J. Org. Chem. 2014, pp. 2415–2428

David Schweinfurth, Naina Deibel, Fritz Weisser, Biprajit Sarkar
Mit Klick zu neuen Liganden [Magazin]
Nachr. Chem. 2011, vol. 59, pp. 937–941

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A product of ChemPubSoc Europe (16 European Chemical Societies)published by Wiley-VCH