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The Chemical Record

Changing Perspectives on the Strategic use of Microwave Heating in Organic Synthesis

Published: 18 October 2017

Author(s): Gregory B. Dudley, A. E. Stiegman

Abstract This Personal Account describes collaborative investigations into apocryphal microwave effects in organic chemistry. Focused research on microwave‐assisted organic synthesis has been fraught with confusion, controversy, and misinformation. Microwave heating is an undoubtedly useful tactic for organic synthesis, but whether or not it can offer strategic advantages remains an open question in the minds of many people....

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European Journal of Lipid Science and Technology

Commentary: New Meta‐Analysis Confirms the Long Established Triacylglycerol‐Lowering Effect of Omega‐3 Fatty Acids Given in Supplemental Form

Published: 18 October 2017

Author(s): Philip C. Calder

thumbnail image: European Journal of Lipid Science and Technology

European Journal of Lipid Science and Technology

Use of Omega‐3 Fatty Acid Supplements Has Insufficient Clinical Evidence for Treatment of Hypertriglyceridemia: A Meta‐Analysis of Randomized, Double‐Blind, Placebo‐Controlled Trials

Published: 18 October 2017

Author(s): Gina E. Nam, Seung‐Kwon Myung, Yoon‐Jung Choi

Omega‐3 fatty acid supplements have been used to treat dyslipidemia. However, there is no comprehensive meta‐analysis of randomized, double‐blind, placebo‐controlled trials that encompasses a broad range of populations with or without underlying diseases regarding their efficacy. PubMed, EMBASE, and Cochrane Library were searched for trials in June 2016. A pooled weighted mean difference with its 95% confidence...

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The Canadian Journal of Chemical Engineering

Direct numerical simulation of turbulent flow over wide‐rib rectangular grooves

Published: 18 October 2017

Author(s): Chonghai Huang, Qinghui Wang, Jinjia Wei, Bo Yu

The turbulent flow over the wide‐rib rectangular grooves, the motions and variations of near‐wall streamwise vortices with time, and the interaction between microgroove and near‐wall streamwise vortices were investigated by direct numerical simulation method (DNS). The distributions of radius, density, and swirling strength of streamwise vortex were also studied quantitatively by using swirling‐strength criterion. It...

thumbnail image: The Canadian Journal of Chemical Engineering

The Canadian Journal of Chemical Engineering

Large‐scale oxidation of multi‐walled carbon nanotubes in fluidized bed from ozone‐containing gas mixtures

Published: 18 October 2017

Author(s): Pierre Lassègue, Laure Noé, Jean‐Charles Dupin, Marc Monthioux, Brigitte Caussat

Abstract 100 g of multi‐walled carbon nanotubes (MWCNTs) tangled in balls of 388 μm in Sauter diameter were treated per run in a pre‐industrial scale fluidized bed reactor, using ozone‐based gaseous mixtures at ambient temperature. The influence of ozone concentration and of the addition of water vapour was studied, for treatment durations between 1 h and 20 h. The process behaviour was analyzed in terms of...

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Advanced Synthesis & Catalysis

Iridium‐Catalyzed Regio‐ and Stereoselective C‐H Oxidative Reaction to ( Z )‐3‐Arylidene‐2‐oxindole Imides under Neutral Conditions

Published: 18 October 2017

Author(s): Zhikai Tu, Jie Tan, Zhiyuan Chen, Tao Tu

Abstract Unsymmetrical 3‐arylidene‐2‐oxindoles are useful pharmacophores for many clinical drugs or intermediates in alkaloids synthesis. An IridiumIII‐catalyzed sequential C−H oxidative reaction of 2‐indolyl enamides has been established. This protocol utilized α,α‐dimethyl benzylhydroperoxide as the oxidant and silver fluoride as a key promoter, to provide a wide range of (Z)‐3‐arylidene‐2‐oxindole imides in moderate to good yields, together with good...

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Propellants, Explosives, Pyrotechnics

A Low‐Sensitivity Composition Based on FOX‐7

Published: 18 October 2017

Author(s): Amel Belaada, Waldemar A. Trzciński, Zbigniew Chyłek, Józef Paszula

Abstract 1,1‐Diamino‐2,2‐dinitroethene (DADNE, FOX‐7) is considered to be an explosive combining comparatively high performance and low sensitivity. In the present study, FOX‐7 has been evaluated as a possible replacement of RDX in TNT‐based melt‐cast compositions. A composition containing FOX‐7, TNT, Al and wax, and a method of preparing it were proposed. Its sensitivity to impact, friction, shock wave, jet impact, fast heating,...

thumbnail image: Propellants, Explosives, Pyrotechnics

Israel Journal of Chemistry

Alkane Carbon‐Hydrogen Bond Functionalization as a Tool Toward a Steric Parameter for Hydrotris(pyrazolyl)borate (Tp x ) Ligands

Published: 18 October 2017

Author(s): Ana Caballero, Pedro J. Pérez

Abstract The effect of a series of hydrotris(pyrazolyl)borate ligands (Tpx) in the regioselectivity of the catalytic functionalization of the secondary carbon‐hydrogen bonds of hexane with ethyl diazoacetate and TpxCuL as the catalysts has led to the definition of the relative steric parameter SPR. The validity of the parameter has been assessed upon its correlation with the regioselectivity observed in several transformations (olefin...

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Chemical Engineering & Technology

Surface Modification of Polysulfone Membranes Using Poly(Acrylic Acid)‐Decorated Alumina Nanoparticles

Published: 18 October 2017

Author(s): Negin Ghaemi, Parisa Daraei, Shiva Palani

Abstract Alumina nanoparticles were decorated with poly(acrylic acid) (PAA) as a hydrophilic polymer by thermal polymerization of acrylic acid in the presence of alumina nanoparticles. The obtained PAA‐decorated alumina (PAA‐d‐Al) nanoparticles were embedded in the polysulfone membrane matrix via nanofiller dispersion in the casting solution. The prepared membranes were characterized by porosity and water contact angle measurements,...

thumbnail image: Chemical Engineering & Technology

Chemical Engineering & Technology

Optimization of a Micromixer with Two‐Layer Serpentine Crossing Channels at Multiple Reynolds Numbers

Published: 18 October 2017

Author(s): Shakhawat Hossain, Kwang-Yong Kim

Abstract Multiobjective optimizations of a micromixer with two‐layer serpentine crossing channels were performed at two different Reynolds numbers by using a multiobjective genetic algorithm and surrogate modeling based on a Navier‐Stokes analysis. The optimizations included three dimensionless design variables, namely, ratios of the diagonal channel width to the pitch length, the main channel width to the pitch length, and the...

thumbnail image: Chemical Engineering & Technology

Most-accessed articles from each ChemPubSoc Europe, ACES, and GDCh journal

September 2017

 


Beau P. Pritchett, Etienne J. Donckele, Brian M. Stoltz
Enantioselective Catalysis Coupled with Stereodivergent Cyclization Strategies Enables Rapid Syntheses of (+)-Limaspermidine and (+)-Kopsihainanine A [Communication]
Angew. Chem. Int. Ed. 2017, vol. 56, p. 12624

Joseph Cowell, Matthew Buck, Ali H. Essa, Rebecca Clarke, Waldemar Vollmer, Daniela Vollmer, Catharien M. Hilkens, John D. Isaacs, Michael J. Hall, Joe Gray
Traceless Cleavage of Protein-Biotin Conjugates under Biologically Compatible Conditions [Communication]
ChemBioChem 2017, vol. 18, p. 1688

Isabela C. Man, Hai-Yan Su, Federico Calle-Vallejo, Heine A. Hansen, José I. Martínez, Nilay G. Inoglu, John Kitchin, Thomas F. Jaramillo, Jens K. Nørskov, Jan Rossmeisl
Universality in Oxygen Evolution Electrocatalysis on Oxide Surfaces [Full Paper]
ChemCatChem 2011, vol. 3, p. 1159

Matthias Ducci
Geheimtinten [Artikel]
Chem. Unserer Zeit 2017, vol. 51, p. 228

Balaram Mukhopadhyay, Rituparna Das
Chemical O-Glycosylations: An Overview [Review]
ChemistryOpen 2016, vol. 5, p. 401

Sigma Hashimoto, Takahiro Iwamoto, Daisuke Kurachi, Eiichi Kayahara, Shigeru Yamago
Shortest Double-Walled Carbon Nanotubes Composed of Cycloparaphenylenes [Communication]
ChemPlusChem 2017, vol. 82, p. 1015

Miaofang Chi, Harry M. Meyer, Zili Wu, Liangbo Liang, Peter V. Bonnesen, Dale K. Hensley, Rui Peng, Yang Song, Cheng Ma, Bobby G. Sumpter, Adam J. Rondinone
High-Selectivity Electrochemical Conversion of CO2 to Ethanol using a Copper Nanoparticle/N-Doped Graphene Electrode [Full Paper]
ChemistrySelect 2016, vol. 1, p. 6055

Ekkehard Schwab, Sebastian Schiebahn, Georg Schaub, Martin Reuter, Konstantin Räuchle, Ludolf Plass, Marcell Peuckert, Anja Metzelthin, Falko Mahlendorf, Wolfram Koch, Renate Hoer, Angelika Heinzel, Sigmar Bräuninger, Martin Bertau, Christian Beilmann, Florian Ausfelder, Ferdi Schüth, Detlef Stolten, Gisa Teßmer, Kurt Wagemann, Karl-Friedrich Ziegahn
Energiespeicherung als Element einer sicheren Energieversorgung [Übersichtsbeitrag]
Chem. Ing. Tech. 2015, vol. 87, p. 17

Abas Mohsenzadeh, Akram Zamani, Mohammad J. Taherzadeh
Bioethylene Production from Ethanol: A Review and Techno-economical Evaluation [Review]
ChemBioEng Rev. 2017, vol. 4, p. 75

Andrzej Kapturkiewicz
Electrochemical Generation of Excited Intramolecular Charge-Transfer States [Review]
ChemElectroChem 2017, vol. 4, p. 1604

Yinghui Xue, Qin Zhang, Tao Zhang, Lei Fu
Black Phosphorus: Properties, Synthesis, and Applications in Energy Conversion and Storage [Focus Review]
ChemNanoMat 2017, vol. 3, p. 352

Reto M. Witzig, Dominik Lotter, Vincent C. Fäseke, Christof Sparr
Stereoselective Arene-Forming Aldol Condensation: Catalyst-Controlled Synthesis of Axially Chiral Compounds [Concept]
Chem. Eur. J. 2017, vol. 23, p. 12960

Sandip G. Agalave, Suleman R. Maujan, Vandana S. Pore
Click Chemistry: 1,2,3‐Triazoles as Pharmacophores [Focus Review]
Chem. Asian J. 2011, vol. 6, p. 2696

Jieun Choi, Nagendra Nath Yadav, Hyun-Joon Ha
Front Cover: Preparation of a Stable Bicyclic Aziridinium Ion and Its Ring Expansion toward Piperidines and Azepanes (Asian J. Org. Chem. 9/2017) [Cover Picture]
Asian J. Org. Chem. 2017, vol. 6, p. 1110

Munia F. Sowaileh, Robert A. Hazlitt, David A. Colby
Application of the Pentafluorosulfanyl Group as a Bioisosteric Replacement [Minireview]
ChemMedChem 2017, vol. 12, p. 1481

Thomas J. Penfold, Andrew P. Monkman, Jamie Gibson
The Importance of Vibronic Coupling for Efficient Reverse Intersystem Crossing in Thermally Activated Delayed Fluorescence Molecules [Communication]
ChemPhysChem 2016, vol. 17, p. 2956

Tugba Ozdemir, Yu-Chen Lu, Safacan Kolemen, Esra Tanriverdi-Ecik, Engin U. Akkaya
Generation of Singlet Oxygen by Persistent Luminescent Nanoparticle-Photosensitizer Conjugates: A Proof of Principle for Photodynamic Therapy without Light [Communication]
ChemPhotoChem 2017, vol. 1, p. 183

Junfei Luo, Igor Larrosa
C−H Carboxylation of Aromatic Compounds through CO2 Fixation [Minireview]
ChemSusChem 2017, vol. 10, p. 3317

Ross J. Marshall, Ross S. Forgan
Postsynthetic Modification of Zirconium Metal-Organic Frameworks [Microreview]
Eur. J. Inorg. Chem. 2016, p. 4310

Gregory J. P. Perry, Igor Larrosa
Recent Progress in Decarboxylative Oxidative Cross-Coupling for Biaryl Synthesis [Microreview]
Eur. J. Org. Chem. 2017, p. 3517

Biochemische und molekularbiologische Analytik [Bericht]
Lebensmittelchemie 2017, vol. 71, p. 13

Maren Bulmahn
Parteien zur Wahl [Bildung & Gesellschaft]
Nachr. Chem. 2017, vol. 65, p. 911

Dominique Rosenberg, Svenja Pansegrau, Mirco Wachholz, Alexander Rehling, Maike Busker, Walter Jansen
Redox-Flow-Batterien - Organische Batterien mit Zukunftsperspektiven [Artikel]
CHEMKON 2017, vol. 24, p. 325

Catharina Goedecke
Why Does Iodine Turn Starch Blue?
ChemViews Magazine 2016

Most cited articles from each ChemPubSoc Europe, ACES, and GDCh journal


2016

 


Shoujun Zhu, Qingnan Meng, Lei Wang, Junhu Zhang, Yubin Song, Han Jin, Kai Zhang, Hongchen Sun, Haiyu Wang, Bai Yang
Highly Photoluminescent Carbon Dots for Multicolor Patterning, Sensors, and Bioimaging
Angew. Chem. Int. Ed. 2013, vol. 52, pp. 3953–3957

Balayeshwanth R. Vummidi, Jawad Alzeer, Nathan W. Luedtke
Fluorescent Probes for G-Quadruplex Structures [Review]
ChemBioChem 2013, vol. 14, pp. 540–558

Zhi-Yuan Gu, Jihye Park, Aaron Raiff, Zhangwen Wei, Hong-Cai Zhou
Metal–Organic Frameworks as Biomimetic Catalysts [Minireview]
ChemCatChem 2014, vol. 6, pp. 67–75

Anthony J. Arduengo, Roland Krafczyk
Auf der Suche nach Stabilen Carbenen [Organische Chemie]
Chem. Unserer Zeit 1998, vol. 32, pp. 6–14

Marc Steinmetz, Stefan Grimme
Benchmark Study of the Performance of Density Functional Theory for Bond Activations with (Ni,Pd)-Based Transition-Metal Catalysts [Full Paper]
ChemistryOpen 2013, vol. 2, pp. 115–124

Philipp Scharf, Jens Müller
Nucleic Acids With Metal-Mediated Base Pairs and Their Applications [Review]
ChemPlusChem 2013, vol. 78, pp. 20–34

Philipp Kaiser, Rajabhau Bajirao Unde, Christoph Kern, Andreas Jess
Production of Liquid Hydrocarbons with CO2 as Carbon Source based on Reverse Water-Gas Shift and Fischer-Tropsch Synthesis [Research Article]
Chem. Ing. Tech. 2013, vol. 85, pp. 489–499

Xiaosi Zhou, Yu-Guo Guo
Highly Disordered Carbon as a Superior Anode Material for Room-Temperature Sodium-Ion Batteries [Communication]
ChemElectroChem 2014, vol. 1, pp. 83–86

Chuanxi Wang, Zhenzhu Xu, Chi Zhang
Polyethyleneimine-Functionalized Fluorescent Carbon Dots: Water Stability, pH Sensing, and Cellular Imaging [Full Paper]
ChemNanoMat 2015, vol. 1, pp. 122–127

Konggang Qu, Jiasi Wang, Jinsong Ren, Xiaogang Qu
Carbon Dots Prepared by Hydrothermal Treatment of Dopamine as an Effective Fluorescent Sensing Platform for the Label-Free Detection of Iron(III) Ions and Dopamine [Full Paper]
Chem. Eur. J. 2013, vol. 19, pp. 7243–7249

Yinuo Wu, Jun Wang, Fei Mao, Fuk Yee Kwong
Palladium-Catalyzed Cross-Dehydrogenative Functionalization of C(sp2)–H Bonds [Focus Review]
Chem. Asian J. 2014, vol. 9, pp. 26–47

Naohiko Yoshikai, Ye Wei
Synthesis of Pyrroles, Indoles, and Carbazoles through Transition-Metal-Catalyzed C–H Functionalization [Review]
Asian J. Org. Chem. 2013, vol. 2, pp. 466–478

Lluís Ballell, Robert H. Bates, Rob J. Young, Daniel Alvarez-Gomez, Emilio Alvarez-Ruiz, Vanessa Barroso, Delia Blanco, Benigno Crespo, Jaime Escribano, Rubén González, Sonia Lozano, Sophie Huss, Angel Santos-Villarejo, José Julio Martín-Plaza, Alfonso Mendoza, María José Rebollo-Lopez, Modesto Remuiñan-Blanco, José Luis Lavandera, Esther Pérez-Herran, Francisco Javier Gamo-Benito, José Francisco García-Bustos, David Barros, Julia P. Castro, Nicholas Cammack
Fueling Open-Source Drug Discovery: 177 Small-Molecule Leads against Tuberculosis [Full Paper]
ChemMedChem 2013, vol. 8, pp. 313–321

Peter Politzer, Jane S. Murray
Halogen Bonding: An Interim Discussion [Review]
ChemPhysChem 2013, vol. 14, pp. 278–294

Volker Hessel, Dana Kralisch, Norbert Kockmann, Timothy Noël, Qi Wang
Novel Process Windows for Enabling, Accelerating, and Uplifting Flow Chemistry [Review]
ChemSusChem 2013, vol. 6, pp. 746–789

Helena J. Shepherd, Gábor Molnár, William Nicolazzi, Lionel Salmon, Azzedine Bousseksou
Spin Crossover at the Nanometre Scale [Microreview]
Eur. J. Inorg. Chem. 2013, pp. 653–661

Junichiro Yamaguchi, Kei Muto, Kenichiro Itami
Recent Progress in Nickel-Catalyzed Biaryl Coupling [Microreview]
Eur. J. Org. Chem. 2013, pp. 19–30

David Schweinfurth, Naina Deibel, Fritz Weisser, Biprajit Sarkar
Mit Klick zu neuen Liganden [Magazin]
Nachr. Chem. 2011, vol. 59, pp. 937–941
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