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Biomedical Chromatography

Qualitative and quantitative analysis of major constituents from Dazhu Hongjingtian capsule by UPLC/Q‐TOF‐MS/MS combined with UPLC/QQQ‐MS/MS

Published: 16 January 2017

Author(s): Guang‐Da Liu, Yi‐Wu Zhao, Yan‐Jing Li, Xue‐Jing Wang, Hai‐Hong Si, Wen‐Zhe Huang, Zhen‐Zhong Wang, Shi‐Ping Ma, Wei Xiao

Abstract In this work, a sensitive and efficient method was established and validated for qualitative and quantitative analysis of major bioactive constituents in Dazhu Hongjingtian capsule by liquid chromatography tandem mass spectrometry. A total of 32 compounds were tentatively identified using ultra‐performance liquid chromatography coupled with quadrupole time‐of‐flight mass spectrometry. Furthermore, 12 constituents, namely...

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Biomedical Chromatography

Simultaneous determination of l ‐tetrahydropalmatine and its active metabolites in rat plasma by a sensitive ultra‐high‐performance liquid chromatography with tandem mass spectrometry method and its application in a pharmacokinetic study

Published: 16 January 2017

Author(s): Weihui Wang, Jing Liu, Xiaoning Zhao, Yan Peng, Nannan Wang, David Y.W. Lee, Ronghua Dai

Abstract A sensitive and reliable ultra‐high‐performance liquid chromatography with tandem mass spectrometry (UHPLC–MS/MS) method was developed and validated for simultaneous determination of l‐tetrahydropalmatine (l‐THP) and its active metabolites l‐isocorypalmine (l‐ICP) and L‐corydalmine (l‐CD) in rat plasma. The analytes were extracted by liquid–liquid extraction and separated on a Bonshell ASB C18 column (2.1 × 100 mm; 2.7 μm; Agela) using...

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Biomedical Chromatography

Quantitative determination and evaluation of Paris polyphylla var. yunnanensis with different harvesting times using UPLC‐UV‐MS and FT‐IR spectroscopy in combination with partial least squares discriminant analysis

Published: 16 January 2017

Author(s): Yuan‐Gui Yang, Ji Zhang, Yan‐Li Zhao, Jin‐Yu Zhang, Yuan‐Zhong Wang

Abstract A rapid method was developed and validated by ultra‐performance liquid chromatography–triple quadrupole mass spectroscopy with ultraviolet detection (UPLC‐UV‐MS) for simultaneous determination of paris saponin I, paris saponin II, paris saponin VI and paris saponin VII. Partial least squares discriminant analysis (PLS‐DA) based on UPLC and Fourier transform infrared (FT‐IR) spectroscopy was employed to evaluate Paris...

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Traffic

Distinct complexes of yeast Snx4 family SNX‐BARs mediate retrograde trafficking of Snc1 and Atg27

Published: 16 January 2017

Author(s): Mengxiao Ma, Christopher G. Burd, Richard J. Chi

The yeast SNX4 sub‐family of sorting nexin containing a Bin‐Amphiphysin‐Rvs domain (SNX‐BAR) proteins, Snx4/Atg24, Snx41 and Atg20/Snx42, are required for endocytic recycling and selective autophagy. Here, we show that Snx4 forms 2 functionally distinct heterodimers: Snx4‐Atg20 and Snx4‐Snx41. Each heterodimer coats an endosome‐derived tubule that mediates retrograde sorting of distinct cargo; the v‐SNARE, Snc1, is a cargo of the...

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Biomedical Chromatography

Application of a solvent‐free solid injection technique coupled with GC–MS for discrimination between the secondary metabolites of wild and cultivated South Korean medicinal foods

Published: 16 January 2017

Author(s): Lieu T. B. Truong, A. M. Abd El‐Aty, Hyun Jin Kim, Md. Musfiqur Rahman, Sung‐Woo Kim, Ho‐Chul Shin, Jae‐Han Shim

Abstract Solvent‐free solid injection was applied to differentiate between wild and cultivated South Korean medicinal foods, including dureup (Aralia elata), deodeok (Codonopsis lanceolata) and doraji (Platycodon grandiflorus). A number of compounds were identified in wild and cultivated dureup (53 and 46), deodeok (47 and 51) and doraji (43 and 38). Secondary metabolites, including butanal,2‐methyl‐, β‐caryophyllene, neoclovene, α‐humulene,...

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Asia-Pacific Journal of Chemical Engineering

A simulation approach to achieve the best miscible enrichment in gas flooding and chemical injection process for enhanced oil recovery

Published: 16 January 2017

Author(s): F. Salari Sardari, M.R. Khorsand Movaghar

Abstract The effect of injected gas composition (as minimum miscible enrichment) on minimum miscibility pressure (MMP) and respective oil recovery has been studied through numerical slim tube simulation on a wide range of gas compositions. An initial comparative study on the performances of representative equations of state for predicting MMP in slim tube simulations has proven Peng–Robinson equation of state to provide results with...

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British Journal of Pharmacology

Teasing apart NAD + metabolism in inflammation: commentary on Zhou et al. (2016). Br J Pharmacol 173: 2352–2368.

Published: 16 January 2017

Author(s): Peter Moon, Paras Minhas

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Chemie Ingenieur Technik - CIT

Gewinnung von Indium aus extrem verdünnten LösungenExtraction of Indium from Extremely Diluted Solutions

Published: 16 January 2017

Author(s): Radek Vostal, Ute Šingliar, Peter Fröhlich

Abstract Der Bedarf an Indium steigt mit dem Wachstum der Elektronikbranche, in der es vorwiegend eingesetzt wird. Daher wurde anhand einer Modelllösung, die in ihrer wesentlichen Zusammensetzung dem Erz Sphalerit entsprach, ein mehrstufiges Extraktionsverfahren zur Gewinnung von Indium entwickelt. Die ursprünglich sehr niedrige Indiumkonzentration in der Lösung wurde durch mehrere aufeinanderfolgende Extraktions‐ und...

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Chemie Ingenieur Technik - CIT

Rückgewinnung von Gadolinium aus pharmazeutischen Abwässern mittels gepulster elektrischer EntladungGadolinium Recovery from Aqueous Pharmaceutical Residuals by Pulsed Electrical Discharge

Published: 16 January 2017

Author(s): Tom Lorenz, Martin Seifert, Karin Jacob‐Seifert, Peter Fröhlich

Abstract Advanced Oxidation Process (AOP) steht für eine In‐situ‐Oxidation, bei der reaktive Sauerstoffspezies durch eine Folge gepulster Plasmaentladungen im wässrigen Medium erzeugt werden. Im Gegensatz zu Verfahren bei denen Ozon durch äußere UV‐Strahler generiert wird, eignet sich der AOP auch für trübe Medien. Aktuell wird der AOP zur Reinigung von chemisch belasteten Abwässern eingesetzt. In dieser Arbeit dient der AOP zum...

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Macromolecular Materials and Engineering

Palladium Nanocubes Assembled Electrospun Nanofiber Membrane: Facile Preparation and Catalytic Properties

Published: 16 January 2017

Author(s): Zhicheng Liu, Zhaodong Yan, Jian Guo, Lu Bai, Lu Jia, Ping Song, Linyu Mei, Yaqing Liu

Assembly of anisotropic nanoparticles on polymeric templates has attracted much attention recently because of the potential useful applications. In this work, 3D electrospun nanofiber membrane is used as template for the assembly of ex situ synthesized palladium nanocubes. The assembly process is achieved by simple immersion step, in which the electrostatic assembly of the nanocubes occurs. The dense nanocubes on the nanofibers as well as...

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Most-accessed articles from each ChemPubSoc Europe, ACES, and GDCh journal

December 2016

 


Thomas Scattolin, Kristina Deckers, Franziska Schoenebeck
Efficient Synthesis of Trifluoromethyl Amines through a Formal Umpolung Strategy from the Bench‐Stable Precursor (Me4N)SCF3 [Communication]
Angew. Chem. Int. Ed. 2017, vol. 56, p. 221

Alex R. Maolanon, Helle M. E. Kristensen, Luke J. Leman, M. Reza Ghadiri, Christian A. Olsen
Natural and Synthetic Macrocyclic Inhibitors of the Histone Deacetylase Enzymes [Review]
ChemBioChem 2017, vol. 18, p. 5

Isabela C. Man, Hai‐Yan Su, Federico Calle‐Vallejo, Heine A. Hansen, José I. Martínez, Nilay G. Inoglu, John Kitchin, Thomas F. Jaramillo, Jens K. Nørskov, Jan Rossmeisl
Universality in Oxygen Evolution Electrocatalysis on Oxide Surfaces [Full Paper]
ChemCatChem 2011, vol. 3, p. 1159

Dieter Wöhrle
Kampf‐ und Explosivstoffe [Treffpunkt Forschung]
Chem. Unserer Zeit 2016, vol. 50, p. 369

Thammadihalli Nanjundaiah Ravishankar, Thippeswamy Ramakrishnappa, Ganganagappa Nagaraju, Hanumanaika Rajanaika
Synthesis and Characterization of CeO2 Nanoparticles via Solution Combustion Method for Photocatalytic and Antibacterial Activity Studies [Full Paper]
ChemistryOpen 2015, vol. 4, p. 146

Andrea Liscio, Konstantinos Kouroupis‐Agalou, Alessandro Kovtun, Elias Gebremedhn, Mohamed El Garah, Wassima Rekab, Emanuele Orgiu, Loris Giorgini, Paolo Samorì, David Beljonne, Vincenzo Palermo
Exfoliation of Few‐Layer Graphene in Volatile Solvents Using Aromatic Perylene Diimide Derivatives as Surfactants [Full Paper]
ChemPlusChem 2016, 10.1002/cplu.201600503

Yang Song, Rui Peng, Dale K. Hensley, Peter V. Bonnesen, Liangbo Liang, Zili Wu, Harry M. Meyer, Miaofang Chi, Cheng Ma, Bobby G. Sumpter, Adam J. Rondinone
High‐Selectivity Electrochemical Conversion of CO2 to Ethanol using a Copper Nanoparticle/N‐Doped Graphene Electrode [Full Paper]
ChemistrySelect 2016, 10.1002/slct.201601169

Florian Ausfelder, Christian Beilmann, Martin Bertau, Sigmar Bräuninger, Angelika Heinzel, Renate Hoer, Wolfram Koch, Falko Mahlendorf, Anja Metzelthin, Marcell Peuckert, Ludolf Plass, Konstantin Räuchle, Martin Reuter, Georg Schaub, Sebastian Schiebahn, Ekkehard Schwab, Ferdi Schüth, Detlef Stolten, Gisa Teßmer, Kurt Wagemann, Karl‐Friedrich Ziegahn
Energiespeicherung als Element einer sicheren Energieversorgung [Übersichtsbeitrag]
Chem. Ing. Tech. 2015, vol. 87, p. 17

Vida Zargar, Morteza Asghari, Amir Dashti
A Review on Chitin and Chitosan Polymers: Structure, Chemistry, Solubility, Derivatives, and Applications [Review]
ChemBioEng Rev. 2015, vol. 2, p. 204

Hanan Al‐Kutubi, Jorge Gascon, Ernst J. R. Sudhölter, Liza Rassaei
Electrosynthesis of Metal–Organic Frameworks: Challenges and Opportunities [Review]
ChemElectroChem 2015, vol. 2, p. 462

Changsoon Choi, Moon Kee Choi, Taeghwan Hyeon, Dae‐Hyeong Kim
Nanomaterial‐Based Soft Electronics for Healthcare Applications [Focus Review]
ChemNanoMat 2016, 10.1002/cnma.201600191

Marco Simonetti, Diego M. Cannas, Adyasha Panigrahi, Szymon Kujawa, Michal Kryjewski, Pan Xie, Igor Larrosa
Ruthenium‐Catalyzed C−H Arylation of Benzoic Acids and Indole Carboxylic Acids with Aryl Halides [Communication]
Chem. Eur. J. 2016, 10.1002/chem.201605068

Yasuhide Inokuma, Kazuki Matsumura, Shota Yoshioka, Makoto Fujita
Finding a New Crystalline Sponge from a Crystallographic Database [Communication]
Chem. Asian J. 2016, 10.1002/asia.201601551

Naoki Asari, Yusuke Takemoto, Yukino Shinomoto, Takuma Yagyu, Akira Yoshimura, Viktor V. Zhdankin, Akio Saito
Cover Picture: Catalytic Cycloisomerization–Fluorination Sequence of N‐Propargyl Amides by Iodoarene/HF⋅Pyridine/Selectfluor Systems (Asian J. Org. Chem. 11/2016) [Cover Picture]
Asian J. Org. Chem. 2016, vol. 5, p. 1295

Hilmar Weinmann
Cancer Immunotherapy: Selected Targets and Small‐Molecule Modulators [Review]
ChemMedChem 2016, vol. 11, p. 450

Chuyang Cheng, J. Fraser Stoddart
Wholly Synthetic Molecular Machines [Minireview]
ChemPhysChem 2016, vol. 17, p. 1780

Jahangir Masud, Polydoros‐Chrysovalantis Ioannou, Nikolaos Levesanos, Panayotis Kyritsis, Manashi Nath
A Molecular Ni‐complex Containing Tetrahedral Nickel Selenide Core as Highly Efficient Electrocatalyst for Water Oxidation [Cover Profile]
ChemSusChem 2016, vol. 9, p. 3123

Ross J. Marshall, Ross S. Forgan
Postsynthetic Modification of Zirconium Metal‐Organic Frameworks [Microreview]
Eur. J. Inorg. Chem. 2016, 10.1002/ejic.201600394

Subhadip Maiti, Laxminarayana Burgula, Jyotirmayee Dash
Palladium Catalyzed Pyridine Group Directed RegioselectiveOxidative C‐H Acylation of Carbazoles Using Aldehydes as theAcyl Source [Full Paper]
Eur. J. Org. Chem. 2016, 10.1002/ejoc.201601322

45. Deutscher Lebensmittelchemikertag 2016 in Freising [Tagungen]
Lebensmittelchemie 2016, vol. 70, p. 157

Rainer Herges
Molekulare Maschinen [Wissenschaft & Forschung]
Nachr. Chem. 2016, vol. 64, p. 1045

Stefan Schwarzer, Ramzy Abdelaziz, Mady Elbahri, Timm Wilke
Wenn ein Wassertropfen zum Nanolabor wird [Das Experiment]
CHEMKON 2016, vol. 23, p. 188

Sarah Millar
Tips and Tricks for the Lab: Column Choices
ChemViews Magazine 2012.

Most Cited articles from ChemPubSoc Europe, ACES, and GDCh journals


2015

 


Shoujun Zhu, Qingnan Meng, Lei Wang, Junhu Zhang, Yubin Song, Han Jin, Kai Zhang, Hongchen Sun, Haiyu Wang, Bai Yang
Highly Photoluminescent Carbon Dots for Multicolor Patterning, Sensors, and Bioimaging
Angew. Chem. Int. Ed. 2013, vol. 52, pp. 3953–3957

Naohiko Yoshikai, Ye Wei
Synthesis of Pyrroles, Indoles, and Carbazoles through Transition-Metal-Catalyzed C–H Functionalization [Review]
Asian J. Org. Chem. 2013, vol. 2, pp. 466–478

Yinuo Wu, Jun Wang, Fei Mao, Fuk Yee Kwong
Palladium-Catalyzed Cross-Dehydrogenative Functionalization of C(sp2)–H Bonds [Focus Review]
Chem. Asian J. 2014, vol. 9, pp. 26–47

Konggang Qu, Jiasi Wang, Jinsong Ren, Xiaogang Qu
Carbon Dots Prepared by Hydrothermal Treatment of Dopamine as an Effective Fluorescent Sensing Platform for the Label-Free Detection of Iron(III) Ions and Dopamine [Full Paper]
Chem. Eur. J. 2013, vol. 19, pp. 7243–7249

Philipp Kaiser, Rajabhau Bajirao Unde, Christoph Kern, Andreas Jess
Production of Liquid Hydrocarbons with CO2 as Carbon Source based on Reverse Water-Gas Shift and Fischer-Tropsch Synthesis [Research Article]
Chem. Ing. Tech. 2013, vol. 85, pp. 489–499

Anthony J. Arduengo, Roland Krafczyk
Auf der Suche nach Stabilen Carbenen [Organische Chemie]
Chem. Unserer Zeit 1998, vol. 32, pp. 6–14

Balayeshwanth R. Vummidi, Jawad Alzeer, Nathan W. Luedtke
Fluorescent Probes for G-Quadruplex Structures [Review]
ChemBioChem 2013, vol. 14, pp. 540–558

Ashish Kumar Singh, Qiang Xu
Synergistic Catalysis over Bimetallic Alloy Nanoparticles [Review]
ChemCatChem 2013, vol. 5, pp. 652–676

Xiaosi Zhou, Yu-Guo Guo
Highly Disordered Carbon as a Superior Anode Material for Room-Temperature Sodium-Ion Batteries [Communication]
ChemElectroChem 2014, vol. 1, pp. 83–86

Marc Steinmetz, Stefan Grimme
Benchmark Study of the Performance of Density Functional Theory for Bond Activations with (Ni,Pd)-Based Transition-Metal Catalysts [Full Paper]
ChemistryOpen 2013, vol. 2, pp. 115–124

Lluís Ballell, Robert H. Bates, Rob J. Young, Daniel Alvarez-Gomez, Emilio Alvarez-Ruiz, Vanessa Barroso, Delia Blanco, Benigno Crespo, Jaime Escribano, Rubén González, Sonia Lozano, Sophie Huss, Angel Santos-Villarejo, José Julio Martín-Plaza, Alfonso Mendoza, María José Rebollo-Lopez, Modesto Remuiñan-Blanco, José Luis Lavandera, Esther Pérez-Herran, Francisco Javier Gamo-Benito, José Francisco García-Bustos, David Barros, Julia P. Castro, Nicholas Cammack
Fueling Open-Source Drug Discovery: 177 Small-Molecule Leads against Tuberculosis [Full Paper]
ChemMedChem 2013, vol. 8, pp. 313–321

Peter Politzer, Jane S. Murray
Halogen Bonding: An Interim Discussion [Review]
ChemPhysChem 2013, vol. 14, pp. 278–294

Philipp Scharf, Jens Müller
Nucleic Acids With Metal-Mediated Base Pairs and Their Applications [Review]
ChemPlusChem 2013, vol. 78, pp. 20–34

Volker Hessel, Dana Kralisch, Norbert Kockmann, Timothy Noël, Qi Wang
Novel Process Windows for Enabling, Accelerating, and Uplifting Flow Chemistry [Review]
ChemSusChem 2013, vol. 6, pp. 746–789

Helena J. Shepherd, Gábor Molnár, William Nicolazzi, Lionel Salmon, Azzedine Bousseksou
Spin Crossover at the Nanometre Scale [Microreview]
Eur. J. Inorg. Chem. 2013, pp. 653–661

Junichiro Yamaguchi, Kei Muto, Kenichiro Itami
Recent Progress in Nickel-Catalyzed Biaryl Coupling [Microreview]
Eur. J. Org. Chem. 2013, pp. 19–30

David Schweinfurth, Naina Deibel, Fritz Weisser, Biprajit Sarkar
Mit Klick zu neuen Liganden [Magazin]
Nachr. Chem. 2011, vol. 59, pp. 937–941
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